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tert-Butyl phenyl carbonate

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tert-Butyl phenyl carbonate Basic information
tert-Butyl phenyl carbonate Chemical Properties
  • Boiling point:83 °C/0.6 mmHg (lit.)
  • Density 1.05 g/mL at 20 °C (lit.)
  • refractive index n20/D 1.480
  • Flash point:214 °F
  • storage temp. Inert atmosphere,Room Temperature
  • form Liquid or Low Melting Solid
  • color Colorless
  • Water Solubility Slightly soluble in water.
  • BRN 2361602
  • NIST Chemistry ReferenceCarbonic acid 1,1-dimethylethyl ester(6627-89-0)
Safety Information
  • Safety Statements 23-24/25
  • WGK Germany 3
  • 21
  • HS Code 29209090
MSDS
tert-Butyl phenyl carbonate Usage And Synthesis
  • Chemical PropertiesClear light yellow liquid
  • Usestert-Butyl phenyl carbonate is used in determination of octanol-water partition coefficients by microemulsion electrokinetic chromatography. It is also used in the synthesis of 2-nitroindoles and as a reagent for mono-Boc protection of α,ω-diamines.
  • Purification MethodsIf IR is free from OH, then purify it by redistillation; otherwise dissolve it in Et2O, wash it with 5% HCl, then H2O, dry it (MgSO4), evaporate and distil it through a Claisen head under vacuum. Care should be taken as distillation of large quantities can lead to decomposition with liberation of CO2 and isobutylene; use the necessary precautions. [Carpino J Am Chem Soc 79 98 1957, Beilstein 6 IV 629.]
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