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N-BROMOACETAMIDE

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N-BROMOACETAMIDE Basic information
N-BROMOACETAMIDE Chemical Properties
  • Melting point:102-105°C
  • Boiling point:127-130 °C(Press: 16 Torr)
  • Density 1.7000 (rough estimate)
  • refractive index 1.4740 (estimate)
  • storage temp. −20°C
  • pka9.41±0.46(Predicted)
  • form powder
  • color white to yellow
  • Water Solubility Soluble in water.
  • Merck 14,1398
  • BRN 969346
  • CAS DataBase Reference79-15-2(CAS DataBase Reference)
  • EPA Substance Registry SystemN-Bromoacetamide (79-15-2)
Safety Information
  • Hazard Codes Xi
  • Risk Statements 36/37/38
  • Safety Statements 26-36
  • RIDADR 3261
  • WGK Germany 3
  • 8
  • TSCA Yes
  • HazardClass 8
  • PackingGroup III
  • HS Code 29299090
MSDS
N-BROMOACETAMIDE Usage And Synthesis
  • General DescriptionWhite powder.
  • Air & Water ReactionsSoluble in water.
  • Reactivity ProfileN-BROMOACETAMIDE is sensitive to light, moisture, and heat. . N-BROMOACETAMIDE decomposes rapidly at elevated temperatures, in the presence of moisture and light.
  • Fire HazardFlash point data are not available for N-BROMOACETAMIDE, but N-BROMOACETAMIDE is probably combustible.
  • Purification MethodsA possible contaminant is CH3CONBr2. Recrystallise it from CHCl3/hexane (1:1, seed if necessary) or water and dry over CaCl2. It is a brominating agent. [Oliveto & Gerold Org Synth Coll Vol IV 104 1963.] Alternatively, dissolve it in the minimum volume of warm H2O (60o), then cool in an ice bath, collect the crystals and dry them in an anhydrous atmosphere, dissolve in Et2O, chill and evaporate till crystallisation. Dry the crystals in vacuo at 25o, then at 45o (m 108o). Crystallise from CHCl3 (m 103o). Estimate the available Br iodometrically [Buckles et al. J Org Chem 23 483 1958]. [Beilstein 2 H 181, 2 I 82, 2 II 180, 2 III 406, 2 IV 417.]
N-BROMOACETAMIDE Preparation Products And Raw materials
N-BROMOACETAMIDE(79-15-2)Related Product Information
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