NISTOSE

25101-99-9

13133-07-8

The general procedure for the synthesis of the target compound from the compound (CAS: 25101-99-9) was as follows: 100 mg of Hex4perAc was dissolved in 5 mL of methanol (MeOH), followed by the addition of 18 mg (0.3 eq.) of sodium methanolate (CH3ONa). After stirring the reaction mixture for 2.5 h at room temperature, Dowex 50Wx2 [H+] resin was added to neutralize the reaction solution. The resin was removed by filtration and the solvent was removed by distillation under reduced pressure. The residue was dissolved in water (H2O) and desalted using a Bio-Gel P-2 gel (10 mL). Finally, a white solid product (57 mg) was obtained by freeze-drying.