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Borane-trimethylamine complex

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Borane-trimethylamine complex Basic information
Borane-trimethylamine complex Chemical Properties
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Borane-trimethylamine complex Usage And Synthesis
  • Chemical Propertieswhite crystalline powder
  • Purification MethodsIt is sublimed using equipment described in Burg and Schlesinger [J Am Chem Soc 59 780 1937I]. Its vapour pressure is 86mm at 100o. It forms colourless hexagonal crystals varying from needles to short lumps, which are slightly soluble in H2O (1.48% at 30o), EtOH (1%), hexane (0.74%) but very soluble in Et2O, *C6H6 and AcOH. It is stable at 125o. [Burg & Schlesinger J Am Chem Soc 59 780 1937, Brown et al. J Am Chem Soc 104 325 1942, Beilstein 4 IV 140.]
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