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Nitrosobenzene

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Nitrosobenzene Basic information
Nitrosobenzene Chemical Properties
  • Melting point:65-69 °C (lit.)
  • Boiling point:59 °C/18 mmHg (lit.)
  • Density 1.1697 (rough estimate)
  • refractive index 1.5389 (estimate)
  • storage temp. 2-8°C
  • BRN 605688
  • Stability:Stable. Incompatible with strong oxidizing agents.
  • InChIKeyNLRKCXQQSUWLCH-UHFFFAOYSA-N
  • CAS DataBase Reference586-96-9
  • NIST Chemistry ReferenceBenzene, nitroso-(586-96-9)
  • EPA Substance Registry SystemNitrosobenzene (586-96-9)
Safety Information
  • Hazard Codes T
  • Risk Statements 20/21-25
  • Safety Statements 26-36/37-45
  • RIDADR UN 2811 6.1/PG 3
  • WGK Germany 3
  • RTECS DA6497525
  • 9-23
  • HazardClass 6.1(b)
  • PackingGroup III
  • HS Code 29042000
MSDS
Nitrosobenzene Usage And Synthesis
  • Chemical Propertieslight yellow solid
  • UsesSpin trap reagent. Has been used in the study of oxidative DNA damage and nitroso-compound-induced respiratory burst in neutrophils3,4.
  • DefinitionChEBI: A nitroso compound that is the nitroso derivative of benzene; a diamagnetic hybrid of singlet O2 and azobenzene.
  • Purification MethodsSteam distil nitrosobenzene, then crystallise it from a small volume of EtOH with cooling below 0o, dry it over CaCl2 in a dessicator at atmospheric pressure, and store it under N2 at 0o. Alternatively it can be distilled onto a cold finger cooled with brine at ~-10o in a vacuum at 17mm (water pump), while heating in a water bath at 65-70o [Robertson & Vaughan J Chem Educ 27 605 1950]. [Beilstein 5 IV 702.]
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