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NYLIDRIN HYDROCHLORIDE

NYLIDRIN HYDROCHLORIDE Structure
NYLIDRIN HYDROCHLORIDE
  • CAS No.849-55-8
  • Chemical Name:NYLIDRIN HYDROCHLORIDE
  • CBNumber:CB6475534
  • Molecular Formula:C19H26ClNO2
  • Formula Weight:335.87
  • MOL File:849-55-8.mol
NYLIDRIN HYDROCHLORIDE Property
  • Melting point 198-199℃ (decomposition)
  • storage temp. Store at -20°C
  • solubility DMSO: ≥ 41 mg/mL (122.07 mM)
  • form Solid
  • color White to Off-White
  • FDA UNII EC69E3PW7E
Safety
  • Hazard Codes  :Xn
  • Risk Statements  :20/21/22
  • Safety Statements  :36
  • WGK Germany  :3
  • RTECS  :DO8300000
Hazard and Precautionary Statements (GHS)
  • Symbol(GHS)
  • Signal wordWarning
  • Hazard statements H332-H312
  • Precautionary statements P280-P302+P352-P312-P322-P363-P501-P261-P271-P304+P340-P312

NYLIDRIN HYDROCHLORIDE Chemical Properties,Usage,Production

  • Chemical Properties White, crystals or powder, odorless; tasteless. Slightly soluble in water and alcohol; very slightly soluble in chloroform, ether; pH of 1% solution is between 4.5 and 6.5.
  • Originator Buphenine hydrochloride,Troponwerke
  • Uses Medicine (treatment of heart disease).
  • Definition ChEBI: Nylidrin hydrochloride is an alkylbenzene.
  • Manufacturing Process The p-benzoxy-α-bromopropiophenone and 1-phenyl-3-amino-butane were heating for an hour on the water bath in the absence of solvents. A solid crystalline cake was obtained. After being extracted with boiling acetic acid, the hydrobromide of 1-(p-hydroxyphenyl)-2-(β-phenylbutylamino)propanone-1 was obtained.
    The hydrobromide of 1-(p-hydroxyphenyl)-2-(β-phenylbutylamino)propanone- 1 was suspended in very pure methanol and shaken with a 10% palladium hydroxide barium sulfate catalyst in contact with, hydrogen. After rather more than 2 mols of hydrogen had been taken-up the hydrogenation stopped. The 1-(p-hydroxyphenyl)-2-(3-phenylbutylamino)propanol-1, was filtered, washed with methanol and evaporated, melting point 110-111°C.
  • Therapeutic Function Vasodilator
NYLIDRIN HYDROCHLORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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NYLIDRIN HYDROCHLORIDE Spectrum
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