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tert-Butyl nitrite

tert-Butyl nitrite Structure
tert-Butyl nitrite
  • CAS No.540-80-7
  • Chemical Name:tert-Butyl nitrite
  • CBNumber:CB6853772
  • Molecular Formula:C4H9NO2
  • Formula Weight:103.12
  • MOL File:540-80-7.mol
tert-Butyl nitrite Property
  • Boiling point: :61-63 °C(lit.)
  • Density  :0.867 g/mL at 25 °C(lit.)
  • refractive index  :n20/D 1.368(lit.)
  • Flash point: :−10 °F
  • storage temp.  :2-8°C
  • solubility  :alcohol: very soluble(lit.)
  • form  :Liquid
  • color  :Clear yellow
  • Water Solubility  :slightly soluble
  • Merck  :14,1583
  • BRN  :1209339
  • CAS DataBase Reference :540-80-7(CAS DataBase Reference)
  • EWG's Food Scores :1
  • FDA UNII :4780H7U8LU
  • NIST Chemistry Reference :(CH3)3CONO(540-80-7)
Safety
  • Hazard Codes  :F,Xn
  • Risk Statements  :11-20/22
  • Safety Statements  :16-24-46
  • RIDADR  :UN 2351 3/PG 2
  • WGK Germany  :1
  • RTECS  :RA0802000
  • F  :8
  • HazardClass  :3
  • PackingGroup  :II
  • HS Code  :29209085
Hazard and Precautionary Statements (GHS)
  • Symbol(GHS)
  • Signal wordDanger
  • Hazard statements H225-H302+H332-H302-H332
  • Precautionary statements P210-P262-P301-P310-P315
tert-Butyl nitrite Price More Price(21)
  • Brand: Sigma-Aldrich
  • Product number: 20370
  • Product name : tert-Butyl nitrite
  • Purity: technical, ≥90% (GC)
  • Packaging: 100ml-f
  • Price: $72.8
  • Updated: 2021/12/16
  • Buy: Buy
  • Brand: Sigma-Aldrich
  • Product number: 20370
  • Product name : tert-Butyl nitrite
  • Purity: technical, ≥90% (GC)
  • Packaging: 100 mL
  • Price: $76
  • Updated: 2021/12/16
  • Buy: Buy
  • Brand: Sigma-Aldrich
  • Product number: 20370
  • Product name : tert-Butyl nitrite
  • Purity: technical, ≥90% (GC)
  • Packaging: 500ml-f
  • Price: $255
  • Updated: 2021/12/16
  • Buy: Buy
  • Brand: Sigma-Aldrich
  • Product number: 20370
  • Product name : tert-Butyl nitrite
  • Purity: technical, ≥90% (GC)
  • Packaging: 500 mL
  • Price: $267
  • Updated: 2021/12/16
  • Buy: Buy
  • Brand: TCI Chemical
  • Product number: N0357
  • Product name : tert-Butyl Nitrite
  • Purity: >90.0%(GC)
  • Packaging: 25mL
  • Price: $49
  • Updated: 2021/12/16
  • Buy: Buy

tert-Butyl nitrite Chemical Properties,Usage,Production

  • Chemical Properties clear yellow liquid
  • Uses Jet propellant.
  • Uses tert-Butyl nitrite is employed as a reagent for diazotization and nitrosation of alcohols, thiols, amines and cycloalkanes. It plays an important role in photocatalyzed conversion of aryl and heteroarylamines to selenides. It finds application in the preparation of aryl azides from aryl amines. It is also useful for radical multifunctionalization reactions of aliphatic alkenes and source of nitric oxide.
  • General Description
    tert-Butyl nitrite (TBN) is an efficient NO source. TBN participates in photocatalyzed conversion of aryl- and heteroarylamines to selenides. It also participates in radical multifunctionalization reactions of aliphatic alkenes.
  • Purification Methods If it is free from OH bands (IR) then distil it through a 12inch helices packed column under reduced pressure, otherwise wash with aqueous 5% NaHCO3 (effervescence), then H2O, dry (Na2SO4) and fractionate it through a 10 theoretical plates column at ca 10mm pressure. [Allen J Chem Soc 1968 1954, Coe & Doumani J Am Chem Soc 70 1516 1948, UV: Ungnade & Smiley J Org Chem 21 993 1956, IR: Terte Bull Soc Chim Belg 60 240 1951, Beilstein 1 IV 1622.]
tert-Butyl nitrite Preparation Products And Raw materials
Raw materials
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