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1,4,5,8-Tetrakis(chloromethyl)naphthalene

产品名称 1,4,5,8-Tetrakis(chloromethyl)naphthalene

CAS号

分子式C14H12Cl4

分子量322.05708

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  • Mass

    MS-IW-2023          
    1,4,5,8-tetrakis(chloromethyl)naphthalene
    C14H12Cl4           (Mass of molecular ion:    320)
    

       Source Temperature: 170 °C
       Sample Temperature: 160 °C
       Direct, 75 eV
    

          35.0       1.0
          36.0      14.6
          38.0       4.7
          39.0       1.4
          50.0       1.5
          51.0       2.5
          62.0       1.6
          63.0       6.7
          74.0       2.1
          75.0       7.0
          75.5       2.1
          76.0      22.2
          76.5       3.0
          77.0       1.6
          81.0       1.8
          81.5       2.6
          82.0       4.7
          82.5       2.9
          87.0       3.1
          87.5       1.6
          88.0      21.4
          88.5       6.8
          89.0      25.6
          89.5       4.8
          90.0       1.4
          93.0       1.9
          99.0       1.2
          99.5       1.1
         100.0       1.4
         105.0       1.0
         106.0       9.3
         106.5       2.8
         107.0       7.0
         107.5       1.5
         108.0       1.5
         115.0       1.3
         124.0       1.8
         125.0       1.7
         126.0       1.6
         127.0       1.0
         139.0       2.1
         149.0       1.0
         150.0       4.4
         151.0       8.4
         152.0      14.0
         153.0       5.5
         163.0       4.2
         164.0       4.6
         165.0      49.4
         166.0      17.8
         167.0       3.4
         174.0       1.2
         175.0       1.9
         176.0      15.1
         177.0      14.1
         178.0      34.9
         179.0      45.5
         180.0      16.8
         181.0       2.8
         198.0       1.0
         199.0       5.9
         200.0       3.8
         201.0       5.2
         202.0       2.6
         203.0       1.5
         209.0       1.0
         211.0       5.2
         212.0       9.5
         213.0      25.3
         214.0      13.7
         215.0      48.6
         216.0      10.8
         217.0      14.1
         218.0       2.2
         236.0       1.9
         238.0       1.2
         244.0       1.1
         249.0      21.1
         250.0      46.5
         251.0      20.6
         252.0      30.2
         253.0       7.0
         254.0       5.4
         271.0       1.0
         285.0     100.0
         286.0      16.3
         287.0      97.9
         288.0      15.3
         289.0      32.0
         290.0       5.0
         291.0       3.7
         320.0      40.0
         321.0       6.2
         322.0      51.7
         323.0       8.1
         324.0      25.4
         325.0       3.8
         326.0       5.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C14 H12 Cl4 0.010 g : 0.5 ml CDCl3
    1,4,5,8-tetrakis(chloromethyl)naphthalene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.632 B 5.281

         Hz     ppm     Int.
    

       3050.78   7.634    599
       2111.45   5.284   1000
       2107.54   5.274     44
    

in CDCl3



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