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MS-NW-7719 1-methyl-2-phenylcyclohexanol C13H18O (Mass of molecular ion: 190)
Source Temperature: 270 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 1.5 18.0 1.2 27.0 5.9 28.0 1.8 29.0 3.2 31.0 1.1 39.0 8.0 40.0 1.0 41.0 8.8 43.0 58.3 44.0 1.7 45.0 2.7 50.0 1.7 51.0 6.2 52.0 1.9 53.0 3.0 54.0 1.0 55.0 3.6 57.0 2.0 58.0 22.7 59.0 4.9 63.0 3.3 64.0 1.3 65.0 6.6 67.0 1.7 68.0 1.2 69.0 1.5 71.0 75.1 72.0 5.2 75.0 1.0 76.0 1.3 77.0 10.5 78.0 9.1 79.0 6.0 80.0 2.1 81.0 8.6 85.0 3.3 89.0 2.6 90.0 1.2 91.0 100.0 92.0 17.4 93.0 1.6 94.0 2.3 97.0 1.2 99.0 6.0 102.0 1.9 103.0 8.1 104.0 32.7 105.0 13.2 106.0 1.3 107.0 1.8 115.0 11.9 116.0 3.7 117.0 21.2 118.0 4.2 119.0 2.6 120.0 1.0 127.0 1.4 128.0 4.8 129.0 19.1 130.0 79.7 131.0 12.3 132.0 25.4 133.0 3.6 134.0 1.1 143.0 8.9 144.0 4.4 145.0 1.1 147.0 6.4 148.0 1.1 157.0 7.9 158.0 1.2 172.0 68.3 173.0 10.5 174.0 4.7 175.0 3.5 190.0 10.5 191.0 1.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H18 O 0.05 ml : 0.5 ml CDCl3 1-methyl-2-phenylcyclohexanol Assign. Shift(ppm)
A 7.29 B 7.28 C 7.26 D 2.471 E 2.038 F 1.81 G 1.71 J 1.59 K 1.46 L 1.33 M 0.959
Hz ppm Int.
2926.15 7.322 61 2924.93 7.319 49 2924.07 7.317 50 2922.36 7.313 36 2920.17 7.307 108 2918.95 7.304 173 2917.60 7.301 101 2916.50 7.298 85 2915.41 7.295 73 2912.84 7.289 234 2911.74 7.286 359 2910.64 7.283 275 2906.98 7.274 134 2904.79 7.269 467 2904.05 7.267 363 2901.73 7.261 93 2900.02 7.257 337 2898.07 7.252 500 2895.39 7.245 107 2892.94 7.239 148 2891.60 7.236 230 2889.65 7.231 300 2888.31 7.228 187 2887.57 7.226 147 2886.47 7.223 378 2884.89 7.219 69 2883.67 7.216 116 2882.32 7.213 115 2881.23 7.210 263 2878.30 7.203 66 2876.22 7.197 59 2874.39 7.193 88 2872.68 7.188 43 996.34 2.494 58 992.92 2.485 60 983.40 2.461 68 979.98 2.453 67 823.85 2.062 47 820.19 2.053 50 810.67 2.029 55 807.01 2.020 55 738.65 1.849 36 736.82 1.844 42 735.96 1.842 37 734.99 1.840 34 733.76 1.837 32 733.28 1.835 31 730.10 1.827 31 727.54 1.821 55 723.88 1.812 88 721.31 1.805 67 716.80 1.794 38 714.84 1.789 35 712.89 1.784 61 711.06 1.780 57 710.57 1.778 57 709.35 1.775 64 707.03 1.770 33 702.03 1.757 40 698.36 1.748 43 688.96 1.724 36 685.30 1.715 55 671.75 1.681 30 645.63 1.616 65 642.94 1.609 72 640.38 1.603 47 638.92 1.599 47 637.45 1.596 41 636.60 1.593 37 636.35 1.593 37 633.54 1.586 45 632.32 1.583 53 630.74 1.579 44 629.27 1.575 51 627.32 1.570 31 625.73 1.566 30 599.85 1.501 50 586.55 1.468 81 582.40 1.458 62 573.24 1.435 42 542.60 1.358 40 538.94 1.349 53 529.66 1.326 36 526.00 1.317 48 383.42 0.960 1000
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