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MassMS-NW-9937 tributylsilane C12H28Si (Mass of molecular ion: 200)
Source Temperature: 200 °C Sample Temperature: 160 °C Reservoir, 75 eV
27.0 1.2 29.0 2.7 31.0 2.4 41.0 2.0 43.0 6.3 44.0 2.0 45.0 12.2 55.0 5.8 56.0 1.4 57.0 7.3 58.0 7.8 59.0 79.6 60.0 6.0 61.0 2.8 71.0 2.6 72.0 3.8 73.0 23.8 74.0 2.1 83.0 1.4 85.0 6.0 86.0 7.4 87.0 57.5 88.0 5.7 89.0 2.1 99.0 1.5 100.0 1.1 101.0 63.4 102.0 6.7 103.0 2.7 113.0 1.1 114.0 5.2 115.0 7.7 116.0 1.0 142.0 2.6 143.0 100.0 144.0 14.2 145.0 4.3 170.0 3.3 171.0 1.9 198.0 7.2 199.0 3.3 200.0 2.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H28 Si 0.05 ml : 0.5 ml CDCl3 tributylsilane 
Assign. Shift(ppm)
A 3.687 B 1.33 C 0.890 D 0.590
Hz ppm Int.1479.98 3.704 48 1476.81 3.696 107 1473.63 3.688 137 1470.34 3.680 105 1467.16 3.672 46 556.03 1.392 31 552.86 1.384 43 547.97 1.372 75 545.65 1.366 113 545.04 1.364 119 540.53 1.353 251 537.96 1.347 579 536.62 1.343 331 534.79 1.339 502 534.06 1.337 494 530.40 1.328 686 528.20 1.322 367 526.98 1.319 398 525.51 1.315 362 522.34 1.307 284 520.26 1.302 146 519.29 1.300 162 516.36 1.293 79 513.79 1.286 69 510.99 1.279 46 375.98 0.941 34 364.99 0.914 109 362.06 0.906 455 359.74 0.901 283 356.69 0.893 409 355.10 0.889 1000 349.98 0.876 253 347.90 0.871 417 245.12 0.614 200 241.94 0.606 248 239.99 0.601 195 238.77 0.598 206 236.94 0.593 268 234.38 0.587 298 233.03 0.584 236 231.20 0.579 238 229.13 0.574 224 225.95 0.566 176
in CDCl3
liquid film
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