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N-亚硝基二异丁胺

产品名称 N-亚硝基二异丁胺

CAS号997-95-5

分子式C8H18N2O

分子量158.24

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  • Mass

    MS-NW-0696          
    n-nitrosodiisobutylamine
    C8H18N2O            (Mass of molecular ion:    158)
    

       Source Temperature: 200 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       3.5
          18.0       4.2
          27.0      16.7
          28.0       7.0
          29.0      31.2
          30.0      47.9
          31.0       1.1
          32.0       1.0
          39.0      13.7
          40.0       2.2
          41.0      55.8
          42.0      61.6
          43.0      97.5
          44.0       5.5
          53.0       1.4
          54.0       1.1
          55.0      14.7
          56.0      22.6
          57.0     100.0
          58.0       5.1
          68.0       1.2
          70.0       6.2
          71.0       1.1
          72.0       4.7
          73.0      12.8
          74.0       1.0
          84.0      57.4
          85.0      14.1
          86.0      19.0
          87.0       1.4
          99.0       1.2
         103.0      10.0
         115.0      24.6
         116.0       1.8
         141.0       5.1
         158.0       5.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H18 N2 O 0.05 ml : 0.5 ml CDCl3
    N-nitrosodiisobutylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.907 B 3.405 C 2.12 D 2.04 E 0.960 F 0.863 J(A,C)=7.6HZ J(B,D)=7.6HZ J(C,E)=6.7HZ J(D,F)=6.8HZ

         Hz     ppm     Int.
    

       1565.31   3.917    427
       1557.74   3.898    430
       1364.75   3.415    434
       1357.18   3.396    430
        862.43   2.158     30
        855.10   2.140     59
        848.39   2.123     78
        841.67   2.107     63
        834.96   2.090     35
        834.23   2.088     33
        828.98   2.075     34
        828.37   2.073     34
        821.66   2.056     61
        814.94   2.040     79
        808.11   2.023     63
        801.39   2.006     30
        800.66   2.004     31
        386.96   0.969   1000
        380.25   0.952    930
        348.14   0.872    976
        341.31   0.855    919
    

in CDCl3



CCl4 solution



liquid film



4880 A,200 M,liquid