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3,4-二氯硝基苯

产品名称 3,4-二氯硝基苯

CAS号99-54-7

分子式C6H3Cl2NO2

分子量192

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  • Mass

    MS-NW-1663          
    1,2-dichloro-4-nitrobenzene
    C6H3Cl2NO2          (Mass of molecular ion:    191)
    

       Source Temperature: 250 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          18.0       2.5
          30.0      45.6
          35.0       1.0
          36.0       2.0
          37.0       8.9
          38.0       4.7
          39.0       1.3
          46.0       1.0
          47.0       1.5
          49.0       4.9
          50.0      14.9
          51.0       3.1
          54.5       1.0
          60.0       2.1
          61.0       5.6
          62.0       4.7
          63.0       6.0
          71.0       1.0
          72.0       3.5
          73.0      14.6
          74.0      52.2
          75.0      42.8
          76.0       3.1
          83.0       2.1
          84.0      15.1
          85.0      10.0
          86.0       5.5
          87.0       3.5
          88.0       1.0
          97.0       2.6
          98.0       1.3
         107.0       2.2
         108.0       3.4
         109.0      85.4
         110.0      19.0
         111.0      27.3
         112.0       6.0
         119.0       2.1
         121.0       1.3
         124.0       1.2
         126.0       1.4
         133.0      48.6
         134.0       2.8
         135.0      31.2
         136.0       1.8
         137.0       5.0
         144.0       1.5
         145.0     100.0
         146.0       7.4
         147.0      62.3
         148.0       4.4
         149.0      10.2
         161.0      36.0
         162.0       2.5
         163.0      22.9
         164.0       1.5
         165.0       3.8
         175.0       2.0
         177.0       1.3
         191.0      95.9
         192.0       6.9
         193.0      60.7
         194.0       4.3
         195.0      10.0
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H3 Cl2 N O2 0.05 ml : 0.5 ml CDCl3
    1,2-dichloro-4-nitrobenzene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.341 B 8.084 C 7.654 J(A,B)=2.5HZ J(B,C)=8.8HZ

         Hz     ppm     Int.
    

        748.38   8.357    779
        745.88   8.329    919
        730.44   8.156    471
        727.88   8.128    352
        721.63   8.058    678
        719.06   8.029    572
        688.88   7.692   1000
        680.13   7.595    655
    


  • 1H NMR 399.65 MHz
    C6 H3 Cl2 N O2 0.042 g : 0.5 ml CDCl3
    1,2-dichloro-4-nitrobenzene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.351 B 8.095 C 7.656

         Hz     ppm     Int.
    

       3338.75   8.355    922
       3336.18   8.348    965
       3241.33   8.111    528
       3238.65   8.104    496
       3232.42   8.089    571
       3229.86   8.082    557
       3068.12   7.678     22
       3064.09   7.667   1000
       3059.69   7.656     30
       3058.59   7.654     33
       3055.18   7.645    931
    

in CDCl3



CCl4 solution



KBr disc



liquid film



nujol mull



4880 A,100M,powder