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MS-NW-4681 alpha,3,4-trichlorotoluene C7H5Cl3 (Mass of molecular ion: 194)
Source Temperature: 260 °C Sample Temperature: 170 °C Reservoir, 75 eV
36.0 2.2 37.0 1.4 38.0 1.4 39.0 3.5 43.0 2.4 44.0 1.8 49.0 1.2 50.0 3.0 51.0 1.6 61.0 6.4 61.5 2.1 62.0 6.1 63.0 8.1 72.0 1.0 73.0 5.3 74.0 1.4 75.0 2.2 79.0 3.1 79.5 1.2 80.0 1.9 84.0 1.0 85.0 1.4 86.0 1.8 87.0 2.5 89.0 11.0 97.0 3.0 99.0 2.9 109.0 1.0 123.0 11.7 124.0 5.2 125.0 4.7 126.0 1.8 133.0 3.1 135.0 1.9 159.0 100.0 160.0 8.4 161.0 64.2 162.0 5.3 163.0 10.5 193.0 1.7 194.0 18.7 195.0 3.0 196.0 18.0 197.0 1.9 198.0 5.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H5 Cl3 0.02 ml : 0.5 ml CDCl3 alpha,3,4-trichlorotoluene Assign. Shift(ppm)
A 4.505 B 7.221 C 7.42 D 7.48
Hz ppm Int.
670.94 7.492 215 670.44 7.486 220 668.94 7.470 337 668.44 7.464 278 661.25 7.384 406 649.94 7.258 230 649.38 7.251 167 647.94 7.235 191 641.69 7.165 94 639.63 7.142 91 403.50 4.506 1000 401.19 4.480 48
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