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MS-NW-8265 Fast Violet B base C15H16N2O2 (Mass of molecular ion: 256)
Source Temperature: 190 °C Sample Temperature: 140 °C Direct, 75 eV
28.0 1.4 39.0 1.1 41.0 1.3 42.0 1.0 51.0 3.9 53.0 1.2 65.0 1.0 66.0 1.3 67.0 1.0 68.0 1.2 77.0 24.8 78.0 2.0 80.0 2.3 81.0 1.6 92.0 1.0 105.0 43.5 106.0 4.0 107.0 1.4 108.0 3.0 109.0 9.1 110.0 1.3 124.0 1.4 135.0 2.2 136.0 10.6 137.0 1.1 138.0 3.1 151.0 100.0 152.0 10.5 153.0 7.8 241.0 1.4 256.0 72.1 257.0 12.5 258.0 1.3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C15 H16 N2 O2 0.038 g : 0.5 ml DMSO-d6 fast violet b base Assign. Shift(ppm)
A 9.65 B 7.979 C 7.554 D 7.502 E 6.740 F 6.530 G 4.64 J 3.723 K 2.047
Hz ppm Int.
3855.29 9.647 169 3194.12 7.993 205 3187.26 7.976 228 3185.73 7.972 180 3028.72 7.579 34 3021.39 7.561 120 3019.10 7.555 41 3015.59 7.546 70 3014.22 7.543 114 3012.85 7.539 68 3004.76 7.519 183 2998.66 7.504 123 2997.13 7.500 229 2991.79 7.487 45 2990.26 7.483 93 2988.89 7.479 63 2693.79 6.741 298 2610.02 6.531 280 1854.55 4.641 274 1488.04 3.724 1000 818.18 2.048 877
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