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MassMS-NW-3809 2-amino-4-chlorophenol C6H6ClNO (Mass of molecular ion: 143)
Source Temperature: 270 °C Sample Temperature: 180 °C Reservoir, 75 eV
18.0 1.0 27.0 2.2 28.0 5.0 29.0 1.0 37.0 1.6 38.0 2.4 38.5 1.8 39.0 2.9 39.5 4.3 41.0 1.2 49.0 1.4 50.0 4.2 51.0 9.2 52.0 7.5 53.0 7.5 53.5 1.3 54.0 2.5 61.0 1.3 62.0 2.2 63.0 9.3 64.0 1.2 65.0 1.1 71.5 2.8 73.0 1.4 76.0 1.6 78.0 6.0 79.0 2.8 80.0 39.0 81.0 3.3 87.0 2.1 89.0 1.0 90.0 1.8 98.0 2.5 108.0 1.8 109.0 2.3 114.0 14.3 115.0 1.5 116.0 4.8 142.0 13.1 143.0 100.0 144.0 11.1 145.0 30.9 146.0 2.3
90 MHz in DMSO-d6
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1H NMR 89.56 MHz C6 H6 Cl N O 0.039 g : 0.5 ml DMSO-d6 2-amino-4-chlorophenol 
Assign. Shift(ppm)
A 9.2 B 6.601 C 6.598 D 6.386 E 4.8 J(B,D)=8.3 HZ. J(C,D)=2.5 HZ.
Hz ppm Int.822.56 9.185 57 596.94 6.666 430 595.19 6.646 51 592.44 6.616 606 589.88 6.587 857 588.63 6.573 1000 586.50 6.549 76 584.94 6.532 39 584.56 6.528 32 575.63 6.428 591 573.25 6.401 443 570.63 6.372 27 570.25 6.368 28 567.31 6.335 256 564.88 6.308 230 427.69 4.776 118
DMSO-d6
KBr disc
nujol mull
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