-
MassMS-IW-3632 6-chloro-2-benzothiazolamine C7H5ClN2S (Mass of molecular ion: 184)
Source Temperature: 150 °C Sample Temperature: 110 °C Direct, 75 eV
45.0 2.1 50.0 1.3 60.0 1.3 61.0 1.7 62.0 2.9 63.0 7.7 69.0 6.6 70.0 1.2 73.0 1.4 74.0 1.4 75.0 1.2 76.0 1.4 78.5 2.1 79.0 1.6 81.0 2.1 82.0 1.9 92.0 7.4 93.0 3.9 94.0 1.3 95.0 4.1 97.0 1.1 105.0 1.7 106.0 1.5 107.0 4.5 108.0 1.0 120.0 1.3 121.0 1.9 122.0 16.1 123.0 1.4 124.0 1.6 130.0 15.1 131.0 1.3 132.0 5.5 139.0 1.4 142.0 2.1 148.0 1.2 149.0 10.4 150.0 1.1 152.0 1.1 156.0 1.5 157.0 21.4 158.0 2.3 159.0 7.9 183.0 1.2 184.0 100.0 185.0 9.7 186.0 36.5 187.0 3.3 188.0 1.5
400 MHz in DMSO-d6
-
1H NMR 399.65 MHz C7 H5 Cl N2 S 0.035 g : 0.5 ml DMSO-d6 6-chloro-2-benzothiazolamine 
Assign. Shift(ppm)
A 7.779 B 7.64 C 7.323 D 7.233
Hz ppm Int.3110.11 7.783 681 3108.03 7.777 674 3098.51 7.754 22 3098.14 7.753 22 3097.78 7.752 22 3069.46 7.681 22 3067.38 7.676 26 3053.10 7.640 1000 2931.76 7.336 440 2923.22 7.315 675 2895.39 7.245 434 2893.31 7.240 421 2886.84 7.224 285 2884.77 7.219 276
in DMSO-d6
KBr disc
nujol mull
更多供应商
