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网站主页CAS数据库列表 946-02-1更多图谱苯甲酸-4-氯丁酯(946-02-1)核磁图(13CNMR)

苯甲酸-4-氯丁酯

产品名称 苯甲酸-4-氯丁酯

CAS号946-02-1

分子式C11H13ClO2

分子量212.67

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  • Mass

    MS-IW-2208          
    4-chlorobutyl benzoate
    C11H13ClO2          (Mass of molecular ion:    212)
    

       Source Temperature: 220 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          27.0       2.4
          29.0       2.0
          39.0       2.0
          41.0       2.0
          50.0       2.6
          51.0      10.1
          54.0       5.9
          55.0      11.1
          76.0       1.9
          77.0      36.5
          78.0       3.1
          79.0       2.0
          90.0       1.1
          91.0       1.1
         105.0     100.0
         106.0       8.9
         107.0       1.6
         122.0      50.4
         123.0      34.3
         124.0       2.7
         135.0       2.0
         177.0       9.5
         178.0       1.1
         212.0       2.6
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C11 H13 Cl O2 0.05 ml : 0.5 ml CDCl3
    4-chlorobutyl benzoate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.038 B 7.537 C 7.426 D 4.341 E 3.590 F 1.92

         Hz     ppm     Int.
    

       3218.75   8.054     94
       3216.92   8.050    447
       3216.55   8.049    417
       3215.82   8.047    564
       3210.69   8.034    178
       3208.74   8.029    619
       3207.15   8.025    560
       3022.34   7.563     79
       3021.12   7.560    150
       3019.78   7.557     93
       3015.63   7.546    109
       3013.55   7.541    341
       3011.72   7.536    134
       3007.57   7.526    154
       3006.23   7.523    271
       3004.88   7.519    157
       2976.68   7.449    107
       2975.10   7.445    433
       2973.63   7.441    218
       2968.38   7.428    353
       2967.29   7.425    619
       2961.43   7.411    129
       2959.84   7.407    299
       2959.23   7.405    243
       1743.04   4.362     52
       1740.84   4.356    249
       1739.14   4.352    191
       1737.06   4.347    210
       1734.74   4.341    649
       1732.91   4.337    265
       1728.76   4.326    253
       1726.56   4.321     55
       1725.34   4.318     38
       1444.46   3.615     34
       1443.24   3.612     49
       1441.04   3.606    237
       1439.33   3.602    154
       1436.89   3.596    262
       1434.81   3.591    670
       1432.98   3.586    206
       1432.13   3.584    210
       1430.54   3.580    193
       1428.71   3.575    272
       1426.51   3.570     59
        782.35   1.958     38
        781.13   1.955     35
        779.66   1.951     39
        777.83   1.947     77
        773.80   1.937    378
        770.63   1.929    546
        767.58   1.921   1000
        764.28   1.913    544
        761.35   1.906    390
        757.45   1.896     79
        755.37   1.891     41
        754.03   1.887     37
        753.05   1.885     38
    

in CDCl3



liquid film