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MS-NW-1080 2,4-dimethyl-2-imidazoline C5H10N2 (Mass of molecular ion: 98)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 11.9 18.0 1.9 26.0 4.5 27.0 11.6 28.0 24.1 29.0 4.3 30.0 5.5 38.0 1.0 39.0 3.8 40.0 4.0 41.0 10.7 41.5 1.3 42.0 78.8 43.0 5.7 44.0 18.8 52.0 2.6 53.0 1.1 54.0 20.2 55.0 100.0 56.0 23.7 57.0 5.2 68.0 23.2 69.0 46.3 70.0 2.4 81.0 1.3 82.0 1.2 83.0 85.7 84.0 4.8 95.0 1.8 96.0 2.5 97.0 8.5 98.0 49.5 99.0 3.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H10 N2 0.04 ml : 0.5 ml CDCl3 2,4-dimethyl-2-imidazoline Assign. Shift(ppm)
A 7.43 B 3.9 C 3.637 D 3.133 E 1.904 F 1.189
Hz ppm Int.
665.00 7.426 1000 355.38 3.969 36 354.69 3.961 40 348.38 3.890 63 342.56 3.825 60 339.44 3.791 82 338.81 3.784 73 329.44 3.679 117 328.63 3.670 110 320.00 3.574 63 319.19 3.564 67 288.50 3.222 72 287.94 3.216 79 281.69 3.146 74 280.94 3.137 77 278.13 3.106 63 277.44 3.098 62 270.94 3.026 43 171.00 1.910 864 170.25 1.901 857 109.44 1.222 757 106.13 1.186 36 103.25 1.153 701
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