图谱信息 供应商 相关产品
网站主页CAS数据库列表 930-36-9更多图谱1-甲基吡唑(930-36-9)红外图谱(IR1)

1-甲基吡唑

产品名称 1-甲基吡唑

CAS号930-36-9

分子式C4H6N2

分子量82.1

展开


  • Mass

    MS-IW-1321          
    1-methylpyrazole
    C4H6N2              (Mass of molecular ion:     82)
    

       Source Temperature: 230 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          15.0       3.3
          26.0       3.0
          27.0       3.4
          28.0      11.0
          29.0       2.7
          30.0       1.5
          38.0       1.6
          39.0       2.3
          40.0       4.3
          41.0       2.5
          42.0      11.0
          51.0       1.7
          52.0       4.4
          53.0       8.7
          54.0      18.6
          55.0       3.3
          81.0      41.1
          82.0     100.0
          83.0       6.3
    

parameter in CDCl3


  • 1H NMR 300 MHz
    C4 H6 N2 ca 5 wt% in CDCl3
    1-methylpyrazole
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 7.33 D(B) 6.23 D(C) 7.55 J(A,B) 2.0 J(A,C) 0.7 J(B,C) 2.2 D(D) 3.88 TENSMEYER,L.G. & AINSWORTH,C. J.ORG.CHEM. 31, 1878 (1966)

         Hz     ppm     Int.
    

       2266.41   7.555    106
       2265.80   7.553    111
       2264.22   7.547    110
       2263.64   7.545    109
       2200.33   7.334    107
       2199.68   7.332    110
       2198.34   7.328    114
       2197.72   7.326    108
       1871.10   6.237     90
       1868.98   6.230    160
       1866.93   6.223     88
       1164.00   3.880   1000
    



liquid film