图谱信息 供应商 相关产品
网站主页CAS数据库列表 93-26-5更多图谱2-乙酰氨基苯甲醚(93-26-5)质谱(MS)

2-乙酰氨基苯甲醚

产品名称 2-乙酰氨基苯甲醚

CAS号93-26-5

分子式C9H11NO2

分子量165.19

展开


  • Mass

    MS-NW-1552          
    2'-methoxyacetanilide
    C9H11NO2            (Mass of molecular ion:    165)
    

       Source Temperature: 250 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          15.0       7.4
          26.0       1.1
          27.0       2.4
          28.0       1.8
          38.0       2.3
          39.0       5.9
          41.0       2.6
          42.0       1.6
          43.0      29.0
          50.0       3.6
          51.0       9.0
          52.0      15.1
          53.0       6.8
          54.0       1.2
          62.0       1.3
          63.0       4.4
          64.0       3.0
          65.0      14.8
          66.0       2.3
          76.0       1.1
          77.0       4.1
          78.0       4.2
          79.0       3.6
          80.0      43.0
          81.0       2.7
          91.0       1.8
          92.0       8.0
          93.0       3.2
          94.0       3.9
          95.0       2.3
         106.0       1.5
         108.0     100.0
         109.0       7.7
         120.0       1.8
         122.0       1.3
         123.0      74.4
         124.0       6.2
         134.0       1.4
         165.0      48.3
         166.0       5.2
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H11 N O2 0.042 g : 0.5 ml CDCl3
    2'-methoxyacetanilide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.346 B 7.80 C 7.018 D 6.940 E 6.856 F 3.853 G 2.179 C AND D WERE CONFIRMED BY LAOCN PROGRAM.

         Hz     ppm     Int.
    

       3340.45   8.359     56
       3338.87   8.355     57
       3332.52   8.339     59
       3330.93   8.335     58
       2806.88   7.024     62
       2805.30   7.020     60
       2799.07   7.004     52
       2797.36   7.000     49
       2781.37   6.960     66
       2780.88   6.959     66
       2779.91   6.956     76
       2779.42   6.955     71
       2773.32   6.940     98
       2771.97   6.936    105
       2765.87   6.921     45
       2765.38   6.920     47
       2764.40   6.918     45
       2763.92   6.916     41
       2744.38   6.867     93
       2743.04   6.864     85
       2736.33   6.847     71
       2734.99   6.844     66
       1540.16   3.854   1000
        870.97   2.180    664
    


  • 1H NMR 89.56 MHz
    C9 H11 N O2 0.035 g : 0.5 ml CDCl3
    2'-methoxyacetanilide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.181 B 3.861 C 6.77 to 7.15 D 7.8 E 8.34

         Hz     ppm     Int.
    

        742.13   8.287     32
        632.25   7.060     40
        628.75   7.021     45
        628.44   7.017     41
        625.81   6.988    127
        625.38   6.983    132
        622.81   6.955     94
        621.63   6.941     45
        619.06   6.913     97
        617.25   6.893    100
        614.63   6.863     48
        614.13   6.858     47
        345.81   3.862   1000
        195.31   2.181    991
    

in CDCl3



KBr disc



nujol mull