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网站主页CAS数据库列表 91-63-4更多图谱2-甲基喹啉(91-63-4)红外图谱(IR2)

2-甲基喹啉

产品名称 2-甲基喹啉

CAS号91-63-4

分子式C10H9N

分子量143.19

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  • Mass

    MS-NW-0146          
    2-methylquinoline
    C10H9N              (Mass of molecular ion:    143)
    

       Source Temperature: 200 °C
       Sample Temperature:  75 °C
       Reservoir, 75 eV
    

          27.0       1.3
          28.0       1.1
          38.0       1.3
          39.0       4.4
          50.0       5.1
          51.0       6.5
          52.0       1.8
          57.5       1.1
          58.5       3.6
          62.0       2.0
          63.0       4.8
          64.0       1.3
          65.0       1.3
          70.5       1.9
          71.5       3.9
          74.0       2.8
          75.0       5.5
          76.0       4.9
          77.0       4.4
          87.0       1.0
          88.0       1.0
          89.0       3.7
          90.0       2.1
         101.0       5.9
         102.0       3.3
         103.0       1.1
         113.0       1.0
         114.0       1.3
         115.0      14.4
         116.0       6.6
         117.0       3.5
         128.0      14.6
         129.0       2.4
         140.0       2.2
         141.0       1.4
         142.0      11.2
         143.0     100.0
         144.0      11.3
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H9 N 24.5 mg : 0.5 ml CDCl3
    2-methylquinoline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.03 B 7.759 C 7.677 D 7.475 E 7.271 F 2.745

         Hz     ppm     Int.
    

       3213.26   8.041    203
       3212.77   8.039    202
       3204.96   8.020    224
       3204.47   8.019    218
       3106.20   7.773     71
       3104.49   7.769     82
       3097.78   7.752     86
       3096.31   7.748     88
       3076.66   7.699     48
       3075.32   7.696     44
       3069.82   7.682     57
       3068.36   7.678    103
       3067.02   7.675     44
       3061.40   7.661     48
       3060.06   7.657     51
       2994.75   7.494     58
       2993.77   7.491     55
       2987.79   7.477     55
       2986.69   7.474     94
       2985.47   7.471     55
       2979.74   7.456     42
       2978.52   7.453     41
       2909.79   7.281    151
       2901.37   7.260    138
       1097.29   2.746   1000
    


  • 1H NMR 89.56 MHz
    C10 H9 N 0.024 g : 0.5 ml CDCl3
    2-methylquinoline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.02 B 7.75 C 7.67 D 7.47 E 7.265 F 2.739

         Hz     ppm     Int.
    

        722.50   8.068    147
        714.19   7.975    195
        699.50   7.811     41
        697.81   7.792     46
        695.19   7.763     41
        693.13   7.740     47
        690.13   7.706     97
        687.88   7.681     98
        686.88   7.670     40
        686.25   7.663     37
        680.00   7.593     67
        678.38   7.575     37
        675.06   7.538     75
        673.69   7.523     72
        667.88   7.458     61
        666.75   7.445     53
        666.00   7.437     38
        654.25   7.306    161
        645.88   7.212    116
        245.38   2.740   1000
    

in CDCl3



CCl4 solution



liquid film