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网站主页CAS数据库列表 90-97-1更多图谱4,4'-二氯二苯甲醇(90-97-1)红外图谱(IR1)

4,4'-二氯二苯甲醇

产品名称 4,4'-二氯二苯甲醇

CAS号90-97-1

分子式C13H10Cl2O

分子量253.12

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  • Mass

    MS-NW-9786          
    bis(p-chlorophenyl)methanol
    C13H10Cl2O          (Mass of molecular ion:    252)
    

       Source Temperature: 150 °C
       Sample Temperature:  90 °C
       Direct, 75 eV
    

          17.0       1.2
          18.0       6.3
          29.0       1.0
          50.0       2.7
          51.0       5.0
          63.0       1.6
          74.0       1.4
          75.0       7.1
          76.0       3.8
          77.0      22.8
          78.0       2.6
          81.5       1.1
          82.0       1.7
         105.0       5.6
         111.0      10.9
         112.0      10.2
         113.0      10.9
         114.0       3.9
         115.0       2.5
         139.0     100.0
         140.0      12.5
         141.0      41.9
         142.0       4.7
         143.0       3.3
         151.0       1.0
         152.0       3.9
         153.0       1.7
         163.0       2.3
         164.0       2.2
         165.0       6.2
         166.0       1.0
         199.0       3.4
         200.0       1.1
         201.0       1.5
         217.0      12.1
         218.0       1.8
         219.0       3.9
         235.0       1.8
         237.0       1.1
         251.0       2.9
         252.0      18.6
         253.0       4.5
         254.0      11.9
         255.0       2.0
         256.0       2.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H10 Cl2 O 0.029 g : 0.5 ml CDCl3
    bis(p-chlorophenyl)methanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.292 B 7.258 C 5.744 D 2.5

         Hz     ppm     Int.
    

       2922.61   7.313     40
       2920.65   7.309    303
       2918.46   7.303    140
       2914.31   7.293    203
       2911.99   7.287   1000
       2910.16   7.282    225
       2905.27   7.270    164
       2903.32   7.265    870
       2901.12   7.260    215
       2894.78   7.244    306
       2295.65   5.745    272
    

in CDCl3



KBr disc



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