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MassMS2001-00883WA sparteine C15H26N2 (Mass of molecular ion: 234)
Source Temperature: 230 °C Sample Temperature: 300 °C Reservoir, 70 eV
27.0 1.4 28.0 1.8 29.0 1.8 30.0 1.6 39.0 2.6 41.0 12.6 42.0 6.3 43.0 1.5 44.0 2.3 53.0 2.9 54.0 4.4 55.0 10.8 56.0 4.2 65.0 1.5 66.0 1.1 67.0 6.6 68.0 6.0 69.0 4.5 70.0 5.0 77.0 1.9 79.0 3.0 80.0 4.5 81.0 3.0 82.0 5.6 83.0 7.6 84.0 15.2 85.0 1.0 89.0 1.3 91.0 1.7 92.0 1.0 93.0 2.9 94.0 4.8 95.0 4.4 96.0 10.1 97.0 33.5 98.0 85.0 99.0 5.9 106.0 2.8 107.0 2.0 108.0 5.2 109.0 6.3 110.0 21.0 111.0 4.7 117.0 2.4 120.0 3.4 121.0 2.2 122.0 12.8 123.0 7.1 124.0 10.2 125.0 1.6 132.0 1.2 134.0 16.1 135.0 8.2 136.0 39.8 137.0 100.0 138.0 13.5 139.0 1.3 148.0 7.7 149.0 5.9 150.0 17.3 151.0 8.2 152.0 5.5 160.0 1.1 162.0 3.9 163.0 2.9 164.0 3.3 165.0 3.7 166.0 1.2 174.0 1.0 175.0 1.1 176.0 5.5 177.0 5.4 178.0 3.1 190.0 3.6 191.0 12.5 192.0 5.3 193.0 43.1 194.0 5.9 204.0 2.5 205.0 7.4 206.0 2.6 218.0 1.2 219.0 2.5 231.0 1.3 232.0 3.6 233.0 15.5 234.0 44.5 235.0 7.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C15 H26 N2 0.05 ml : 0.5 ml CDCl3 sparteine 
Assign. Shift(ppm)
A 2.778 B 2.69 C 2.68 D 2.523 E 2.342 F 2.05 G 2.02 J 2.0 K 1.95 L 1.93 M 1.839 N 1.71 P 1.55 Q 1.49 R 1.46 S 1.38 T 1.34 U 1.23 V 1.048 ASSIGNED BY C-H COSY
Hz ppm Int.1116.09 2.793 272 1108.28 2.774 163 1104.98 2.765 294 1104.13 2.763 289 1086.55 2.719 361 1075.56 2.692 1000 1064.58 2.664 712 1016.60 2.544 218 1014.28 2.538 321 1011.96 2.533 230 1005.62 2.517 253 1003.42 2.511 360 1000.98 2.505 252 943.24 2.361 402 939.70 2.352 418 932.13 2.333 354 928.59 2.324 365 828.74 2.074 256 826.90 2.070 258 824.83 2.064 172 822.75 2.059 167 820.92 2.055 164 818.97 2.050 172 816.89 2.045 296 814.70 2.039 378 810.79 2.029 229 805.30 2.016 615 802.73 2.009 780 798.71 1.999 322 794.43 1.988 597 791.87 1.982 603 787.11 1.970 548 783.69 1.961 409 781.74 1.957 390 775.88 1.942 593 771.85 1.932 577 764.77 1.914 191 760.62 1.904 278 742.43 1.858 190 740.60 1.854 234 738.77 1.849 238 736.82 1.844 201 734.38 1.838 181 731.81 1.832 200 729.86 1.827 226 727.91 1.822 220 726.07 1.817 170 693.36 1.735 362 682.01 1.707 757 676.27 1.693 326 671.88 1.682 445 638.67 1.599 260 635.38 1.590 366 630.25 1.578 551 628.78 1.574 449 626.46 1.568 631 622.92 1.559 403 620.12 1.552 408 616.94 1.544 484 615.72 1.541 471 612.55 1.533 521 610.35 1.528 625 606.93 1.519 766 603.15 1.510 403 597.53 1.496 463 595.58 1.491 477 591.80 1.481 195 589.11 1.475 216 586.30 1.468 399 582.76 1.459 489 580.44 1.453 373 561.16 1.405 276 557.25 1.395 244 549.80 1.376 351 546.02 1.367 280 543.82 1.361 158 537.11 1.344 383 534.42 1.338 260 532.59 1.333 200 526.00 1.317 512 521.00 1.304 254 517.70 1.296 378 513.92 1.286 309 504.39 1.263 195 502.69 1.258 249 500.12 1.252 365 498.66 1.248 414 495.97 1.242 352 492.19 1.232 184 487.92 1.221 434 484.74 1.213 413 478.52 1.198 174 473.02 1.184 194 427.37 1.070 261 424.80 1.063 466 422.36 1.057 264 415.41 1.040 259 412.96 1.034 448 410.52 1.028 249
Liquid film
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