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MassMS-NW-0892 1-bromonaphthalene C10H7Br (Mass of molecular ion: 206)
Source Temperature: 280 °C Sample Temperature: 150 °C Reservoir, 75 eV
37.0 1.0 38.0 1.4 39.0 2.0 49.0 1.2 50.0 8.7 51.0 7.4 52.0 1.1 61.0 3.0 62.0 5.2 63.0 20.0 63.5 11.6 64.0 1.6 73.0 1.3 74.0 11.0 75.0 11.9 76.0 6.2 77.0 12.4 85.0 1.1 86.0 2.7 87.0 3.8 90.0 1.7 91.0 1.8 98.0 4.5 99.0 3.7 100.0 2.9 101.0 9.3 102.0 1.1 103.0 8.4 103.5 1.0 104.0 8.3 122.0 1.0 125.0 2.2 126.0 25.4 127.0 100.0 128.0 12.2 206.0 99.2 207.0 11.7 208.0 96.7 209.0 10.7 286.0 1.6
400 MHz in CDCl3
parameter in CCl4
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1H NMR 399.65 MHz C10 H7 Br 0.05 ml : 0.5 ml CDCl3 1-bromonaphthalene 
Assign. Shift(ppm)
A 8.194 B 7.731 C 7.706 D 7.699 E 7.509 F 7.442 G 7.210 ASSIGNED BY C-H COSY
Hz ppm Int.3283.08 8.215 44 3279.17 8.206 511 3275.63 8.197 40 3271.36 8.186 518 3270.39 8.184 551 3097.66 7.751 64 3093.87 7.742 501 3093.26 7.740 471 3088.87 7.729 122 3086.43 7.723 592 3084.84 7.719 960 3083.74 7.717 1000 3081.18 7.710 702 3077.39 7.701 591 3076.29 7.698 986 3072.88 7.689 713 3010.86 7.534 318 3009.64 7.531 328 3004.03 7.517 515 3002.69 7.514 641 3001.10 7.510 360 2997.80 7.502 58 2995.61 7.496 469 2994.26 7.493 472 2993.04 7.490 340 2986.08 7.472 34 2984.99 7.470 36 2981.45 7.461 468 2980.10 7.457 519 2974.49 7.443 329 2973.27 7.440 651 2972.05 7.437 491 2966.31 7.423 289 2965.21 7.420 284 2959.84 7.407 31 2889.04 7.229 689 2885.50 7.221 32 2881.59 7.211 729 2880.86 7.209 779 2873.41 7.190 610
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1H NMR 300 MHz C10 H7 Br 5 mol% in CCl4 1-bromonaphthalene Parameter ppm Hz
D(A) 7.701 D(B) 7.226 D(C) 7.698 D(D) 7.724 D(E) 7.432 D(F) 7.507 D(G) 8.182 J(A,B) 7.2 J(A,C) 1.3 J(A,D) 0.0 J(A,E) 0.0 J(A,F) 0.0 J(A,G) 0.8 J(B,C) 8.3 J(B,D) 0.0 J(B,E) 0.0 J(B,F) 0.0 J(B,G) 0.0 J(C,D) 0.0 J(C,E) 0.0 J(C,F) 0.0 J(C,G) 0.7 J(D,E) 8.2 J(D,F) 0.9 J(D,G) 0.7 J(E,F) 6.7 J(E,G) 0.9 J(F,G) 8.1 EMSLEY,J.W. ET AL. J.CHEM.SOC. B 1970, 1513
Hz ppm Int.2458.69 8.196 253 2450.71 8.169 277 2449.96 8.167 217 2322.23 7.741 206 2321.43 7.738 288 2320.51 7.735 200 2314.15 7.714 951 2313.52 7.712 1000 2306.79 7.689 446 2306.07 7.687 710 2260.35 7.534 136 2259.35 7.531 147 2253.66 7.512 254 2252.60 7.509 308 2251.36 7.505 142 2245.78 7.486 244 2244.66 7.482 216 2236.79 7.456 252 2235.72 7.452 265 2230.10 7.434 156 2228.81 7.429 286 2227.75 7.426 221 2222.04 7.407 127 2221.06 7.404 119 2175.33 7.251 356 2168.05 7.227 345 2167.14 7.224 341 2159.85 7.199 287
in CDCl3
CCl4 solution
liquid film
4880 A,200 M,liquid
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