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网站主页CAS数据库列表 88-95-9更多图谱邻苯二甲酰氯(88-95-9)质谱(MS)

邻苯二甲酰氯

产品名称 邻苯二甲酰氯

CAS号88-95-9

分子式C8H4Cl2O2

分子量203.02

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  • Mass

    MS-NW-5117          
    phthaloyl dichloride
    C8H4Cl2O2           (Mass of molecular ion:    202)
    

       Source Temperature: 260 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          27.0       1.8
          28.0       2.7
          29.0       5.3
          35.0       1.3
          36.0       5.5
          37.0       5.0
          37.5       2.2
          38.0       9.1
          39.0       1.1
          49.0       2.7
          50.0      21.6
          51.0       2.9
          52.0       6.9
          61.0       1.8
          62.0       1.2
          66.0      10.0
          73.0       2.3
          73.5       8.7
          74.5      14.8
          75.5      23.7
          76.5       2.5
          84.0       1.3
         104.0      21.8
         105.0       2.0
         111.0      29.3
         112.0       2.2
         113.0       9.8
         139.0       4.3
         141.0       1.4
         148.0       2.0
         164.0       1.6
         167.0     100.0
         168.0       9.2
         169.0      32.8
         170.0       3.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H4 Cl2 O2 0.05 ml : 0.5 ml CDCl3
    phthaloyl dichloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.940 B 7.787

         Hz     ppm     Int.
    

       3181.76   7.962    172
       3177.98   7.952    853
       3174.68   7.944    798
       3172.12   7.938    795
       3168.95   7.930   1000
       3164.92   7.920    227
       3126.71   7.824     30
       3120.48   7.809    164
       3116.33   7.798    994
       3113.16   7.790    702
       3110.60   7.784    694
       3107.30   7.776    764
       3103.39   7.766     97
       3097.66   7.751     23
       3096.31   7.748     21
    

in CDCl3



liquid film