均三甲苯胺

产品名称均三甲苯胺

CAS号88-05-1

分子式C9H13N

分子量135.21

¹³CNMR

Mass

MS-NW-0756          
2,4,6-trimethylaniline
C9H13N              (Mass of molecular ion:    135)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       1.9
      28.0       2.3
      39.0       4.8
      41.0       2.7
      42.0       2.4
      51.0       2.8
      52.0       1.9
      53.0       2.4
      53.5       1.2
      54.0       1.5
      58.5       1.4
      59.5       1.5
      63.0       1.7
      65.0       4.4
      65.5       2.1
      66.0       1.9
      66.5       1.2
      67.0       1.3
      67.5       3.0
      77.0       5.9
      78.0       1.8
      79.0       3.4
      80.0       1.2
      91.0      10.5
      92.0       2.1
      93.0       2.8
      94.0       1.5
     103.0       2.6
     104.0       1.3
     105.0       2.1
     106.0       2.2
     107.0       1.8
     115.0       3.3
     116.0       1.3
     117.0       4.9
     118.0       4.4
     119.0       4.3
     120.0      76.7
     121.0       7.1
     132.0       2.7
     133.0       2.1
     134.0      60.1
     135.0     100.0
     136.0      10.4

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₉ H₁₃ N	0.04 ml : 0.5 ml CDCl₃
2,4,6-trimethylaniline

    Assign.     Shift(ppm)

      A             6.748
      B             3.40
      C             2.193
      D             2.133

     Hz     ppm     Int.

    604.44   6.749    230
    304.56   3.401     48
    196.50   2.195    493
    191.06   2.134   1000

in CDCl3

CCl4 solution

liquid film

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