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MassMS-IW-9281 1-(triisopropylsilyl)pyrrole C13H25NSi (Mass of molecular ion: 223)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 1.9 39.0 2.0 41.0 3.7 42.0 1.3 43.0 9.6 44.0 2.3 45.0 8.0 53.0 1.7 54.0 1.1 55.0 3.5 57.0 1.1 58.0 1.5 59.0 28.1 60.0 2.3 61.0 1.0 62.0 3.2 66.0 1.1 67.0 9.9 68.0 4.3 69.0 7.6 70.0 2.2 71.0 8.9 72.0 1.7 73.0 6.3 81.0 1.4 82.0 1.8 83.0 13.8 84.0 3.0 85.0 13.9 86.0 1.8 87.0 3.3 94.0 17.6 95.0 5.7 96.0 8.5 97.0 8.5 98.0 1.9 99.0 1.1 109.0 1.9 110.0 33.2 111.0 7.8 112.0 2.0 113.0 4.5 114.0 1.1 122.0 1.5 123.0 1.1 124.0 26.5 125.0 5.1 126.0 1.3 136.0 2.7 137.0 1.1 138.0 25.0 139.0 22.1 140.0 3.7 152.0 43.9 153.0 7.6 154.0 2.1 164.0 1.0 180.0 100.0 181.0 35.6 182.0 7.6 183.0 1.3 222.0 1.6 223.0 42.5 224.0 8.6 225.0 2.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H25 N Si 0.05 ml : 0.5 ml CDCl3 1-(triisopropylsilyl)pyrrole 
Assign. Shift(ppm)
A 6.794 B 6.312 C 1.447 D 1.097
Hz ppm Int.2717.41 6.800 137 2715.45 6.795 184 2713.50 6.790 133 2524.66 6.318 159 2522.71 6.313 205 2520.75 6.308 146 594.60 1.488 46 587.04 1.469 107 579.47 1.450 149 571.90 1.432 125 564.45 1.413 75 448.85 1.124 60 442.26 1.107 1000 434.57 1.088 921 428.34 1.072 68
in CDCl3
liquid film
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