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MassMS-IW-7698 1-butylpyridinium bromide C9H14BrN (Mass of molecular ion: 215)
Source Temperature: 190 °C Sample Temperature: 210 °C Direct, 75 eV
26.0 5.0 27.0 13.7 28.0 8.4 29.0 23.5 37.0 1.3 38.0 2.6 38.5 1.0 39.0 12.6 40.0 1.5 41.0 43.5 42.0 2.0 43.0 3.1 49.0 2.0 50.0 11.1 51.0 20.8 52.0 62.3 53.0 7.4 55.0 5.9 56.0 14.3 57.0 89.5 58.0 4.5 75.0 1.5 76.0 1.2 78.0 13.2 79.0 100.0 80.0 8.5 81.0 1.3 82.0 3.9 107.0 4.4 109.0 4.2 136.0 8.7 138.0 8.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H14 Br N 0.041 g : 0.5 ml CDCl3 1-butylpyridinium bromide 
Assign. Shift(ppm)
A 9.666 B 8.623 C 8.223 D 5.038 E 2.070 F 1.442 G 0.968
Hz ppm Int.3867.19 9.677 223 3865.97 9.674 270 3860.47 9.660 274 3859.10 9.657 238 3455.51 8.647 48 3454.28 8.644 86 3452.91 8.640 51 3447.57 8.627 96 3446.35 8.624 186 3445.13 8.621 98 3439.94 8.608 62 3438.57 8.604 107 3437.35 8.601 60 3293.46 8.241 170 3286.74 8.225 221 3285.83 8.222 214 3278.96 8.205 155 2021.03 5.058 183 2013.55 5.039 299 2006.07 5.020 193 842.44 2.108 50 834.81 2.089 117 832.37 2.083 56 829.47 2.076 86 827.33 2.071 187 824.58 2.064 83 819.70 2.052 125 812.07 2.032 58 596.01 1.492 30 588.53 1.473 112 581.05 1.454 168 573.12 1.435 174 565.64 1.416 119 558.32 1.398 36 394.13 0.987 476 386.81 0.968 1000 379.49 0.950 422
in CDCl3
KBr disc
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