2-吡啶甲醛肟

Mass

MS-NW-1435          
2-pyridinecarbaldehyde oxime
C6H6N2O             (Mass of molecular ion:    122)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      17.0       1.2
      18.0       5.2
      26.0       5.5
      27.0       6.2
      28.0       5.7
      30.0       1.0
      37.0       2.9
      38.0       5.3
      39.0      10.2
      40.0       1.3
      41.0       1.1
      44.0       1.8
      49.0       2.4
      50.0      13.7
      51.0      27.8
      52.0      18.3
      53.0       3.2
      62.0       1.5
      63.0       4.2
      64.0       3.8
      65.0      59.2
      66.0       5.3
      67.0       1.6
      75.0       2.9
      76.0       5.8
      77.0      12.8
      78.0      24.0
      79.0      33.7
      80.0       1.9
      91.0       2.4
      92.0      25.0
      93.0       2.0
      95.0       1.3
     103.0       1.2
     104.0      25.7
     105.0       4.3
     121.0       7.5
     122.0     100.0
     123.0       7.5

Parameter ppm Hz D(A) 8.75 D(B) 7.39 D(C) 7.93 D(D) 7.78 J(A,B) 4.9 J(A,C) 1.8 J(A,D) 1.4 J(B,C) 7.7 J(B,D) 1.0 J(C,D) 8.1 D(E) 8.46 D(F) 12.20 BRUEGEL,W. Z.ELEKTROCHEM.BER.BUNSENGES.PHYS.CHEM. 66, 159 (1962)

     Hz     ppm     Int.

   3660.02  12.200   1000
   2629.06   8.764    152
   2627.50   8.758    241
   2625.89   8.753    167
   2624.15   8.747    169
   2622.59   8.742    247
   2621.03   8.737    159
   2538.00   8.460   1000
   2388.22   7.961    109
   2386.48   7.955    109
   2380.28   7.934    229
   2378.49   7.928    225
   2372.47   7.908    171
   2370.73   7.902    168
   2338.87   7.796    198
   2337.71   7.792    313
   2336.55   7.788    204
   2330.80   7.769    143
   2329.59   7.765    213
   2328.43   7.761    138
   2223.67   7.412    163
   2222.69   7.409    163
   2218.81   7.396    165
   2217.78   7.393    169
   2216.04   7.387    161
   2215.02   7.383    153
   2211.14   7.370    147
   2210.15   7.367    144