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网站主页CAS数据库列表 87-17-2更多图谱水杨酰苯胺(87-17-2)质谱(MS)

水杨酰苯胺

产品名称 水杨酰苯胺

CAS号87-17-2

分子式C13H11NO2

分子量213.23

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  • Mass

    MS-NW-0212          
    salicylanilide
    C13H11NO2           (Mass of molecular ion:    213)
    

       Source Temperature: 190 °C
       Sample Temperature:   0 °C
       Direct, 75 eV
    

          18.0       1.8
          38.0       1.8
          39.0      12.1
          50.0       1.2
          51.0       3.0
          53.0       1.8
          62.0       1.0
          63.0       3.8
          64.0       3.3
          65.0      20.2
          66.0       4.4
          77.0       2.8
          92.0       3.8
          93.0     100.0
          94.0       7.2
         120.0       1.1
         121.0      31.6
         122.0       2.5
         213.0      24.0
         214.0       3.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H11 N O2 0.042 g : 0.5 ml CDCl3
    salicylanilide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 11.99 B 8.08 C 7.53 D 7.52 E 7.410 F 7.356 G 7.175 J 7.000 K 6.878

         Hz     ppm     Int.
    

       4791.63  11.990    647
       3228.68   8.079    149
       3029.76   7.582     30
       3029.21   7.580     31
       3028.29   7.578     37
       3027.01   7.575     40
       3026.46   7.573     38
       3026.09   7.572     38
       3024.99   7.570     40
       3017.67   7.551    506
       3016.39   7.548    645
       3014.55   7.543    225
       3012.91   7.539    105
       3009.79   7.532    604
       3008.88   7.529    936
       3007.78   7.527   1000
       3005.76   7.521    143
       3001.37   7.510    370
       2999.72   7.506    393
       2972.43   7.438     36
       2970.59   7.433    288
       2968.95   7.429    279
       2965.65   7.421     46
       2963.27   7.415    330
       2962.17   7.412    399
       2961.80   7.411    385
       2960.70   7.409    317
       2958.32   7.403     51
       2957.59   7.401     47
       2955.03   7.395    332
       2953.38   7.390    336
       2949.35   7.380    130
       2947.52   7.376    533
       2945.50   7.371    202
       2942.20   7.362    154
       2940.01   7.357    721
       2939.27   7.355    605
       2933.41   7.340    217
       2931.58   7.336    535
       2929.56   7.331     86
       2877.73   7.201     30
       2875.71   7.196    192
       2874.43   7.193    335
       2873.33   7.190    210
       2868.57   7.178    189
       2867.84   7.176    222
       2867.11   7.175    497
       2866.37   7.173    259
       2865.64   7.171    173
       2860.88   7.159    133
       2859.60   7.156    231
       2858.50   7.153    134
       2802.08   7.012    426
       2801.35   7.010    467
       2800.98   7.009    454
       2796.40   6.998     33
       2793.84   6.991    405
       2792.92   6.989    424
       2792.56   6.988    400
       2756.84   6.899    314
       2755.74   6.896    318
       2752.44   6.888     36
       2749.70   6.881    339
       2748.96   6.879    396
       2748.41   6.878    393
       2747.68   6.876    348
       2741.64   6.861    285
       2740.54   6.858    272
    

in CDCl3



KBr disc



nujol mull