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MassMS-NW-0212 salicylanilide C13H11NO2 (Mass of molecular ion: 213)
Source Temperature: 190 °C Sample Temperature: 0 °C Direct, 75 eV
18.0 1.8 38.0 1.8 39.0 12.1 50.0 1.2 51.0 3.0 53.0 1.8 62.0 1.0 63.0 3.8 64.0 3.3 65.0 20.2 66.0 4.4 77.0 2.8 92.0 3.8 93.0 100.0 94.0 7.2 120.0 1.1 121.0 31.6 122.0 2.5 213.0 24.0 214.0 3.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H11 N O2 0.042 g : 0.5 ml CDCl3 salicylanilide 
Assign. Shift(ppm)
A 11.99 B 8.08 C 7.53 D 7.52 E 7.410 F 7.356 G 7.175 J 7.000 K 6.878
Hz ppm Int.4791.63 11.990 647 3228.68 8.079 149 3029.76 7.582 30 3029.21 7.580 31 3028.29 7.578 37 3027.01 7.575 40 3026.46 7.573 38 3026.09 7.572 38 3024.99 7.570 40 3017.67 7.551 506 3016.39 7.548 645 3014.55 7.543 225 3012.91 7.539 105 3009.79 7.532 604 3008.88 7.529 936 3007.78 7.527 1000 3005.76 7.521 143 3001.37 7.510 370 2999.72 7.506 393 2972.43 7.438 36 2970.59 7.433 288 2968.95 7.429 279 2965.65 7.421 46 2963.27 7.415 330 2962.17 7.412 399 2961.80 7.411 385 2960.70 7.409 317 2958.32 7.403 51 2957.59 7.401 47 2955.03 7.395 332 2953.38 7.390 336 2949.35 7.380 130 2947.52 7.376 533 2945.50 7.371 202 2942.20 7.362 154 2940.01 7.357 721 2939.27 7.355 605 2933.41 7.340 217 2931.58 7.336 535 2929.56 7.331 86 2877.73 7.201 30 2875.71 7.196 192 2874.43 7.193 335 2873.33 7.190 210 2868.57 7.178 189 2867.84 7.176 222 2867.11 7.175 497 2866.37 7.173 259 2865.64 7.171 173 2860.88 7.159 133 2859.60 7.156 231 2858.50 7.153 134 2802.08 7.012 426 2801.35 7.010 467 2800.98 7.009 454 2796.40 6.998 33 2793.84 6.991 405 2792.92 6.989 424 2792.56 6.988 400 2756.84 6.899 314 2755.74 6.896 318 2752.44 6.888 36 2749.70 6.881 339 2748.96 6.879 396 2748.41 6.878 393 2747.68 6.876 348 2741.64 6.861 285 2740.54 6.858 272
in CDCl3
KBr disc
nujol mull
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