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氯(二异丙基氨基)甲氧基膦

产品名称 氯(二异丙基氨基)甲氧基膦

CAS号86030-43-5

分子式C7H17ClNOP

分子量197.64


  • Mass

    MS-NW-9542          
    methyl diisopropylphosphoramidochloridite
    C7H17ClNOP          (Mass of molecular ion:    197)
    

       Source Temperature: 240 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       5.1
          18.0       1.1
          27.0       8.3
          28.0       4.0
          29.0       1.6
          30.0       2.3
          31.0       1.2
          36.0       1.9
          39.0       4.4
          40.0       1.0
          41.0      16.5
          42.0      21.7
          43.0      22.3
          44.0      21.0
          45.0       1.3
          46.0      16.2
          47.0      14.5
          48.0       1.3
          49.0       1.2
          50.0       5.8
          52.0       1.9
          56.0       3.0
          58.0      11.8
          59.0       1.9
          62.0       2.6
          63.0      21.2
          64.0       1.0
          67.0       1.1
          70.0       2.9
          72.0       1.9
          73.0       1.9
          74.0       1.8
          78.0      32.4
          79.0       3.4
          80.0       1.4
          82.0       2.1
          84.0      16.0
          85.0       1.2
          86.0       9.7
          88.0      40.4
          89.0       1.7
          90.0       7.9
          93.0      15.8
          94.0       2.7
          96.0       1.4
          97.0      41.4
          98.0       1.6
          99.0      13.5
         100.0       2.2
         104.0      64.7
         105.0       2.8
         108.0      33.6
         109.0       2.8
         110.0      11.6
         118.0       5.5
         120.0      21.2
         121.0       1.0
         122.0      11.3
         124.0       4.6
         126.0       1.1
         128.0       2.5
         130.0       3.0
         131.0       1.0
         132.0       3.9
         136.0       3.7
         140.0      52.5
         141.0       2.4
         142.0      17.4
         146.0       1.1
         147.0       1.5
         150.0       2.3
         152.0       2.6
         154.0       2.7
         156.0      16.5
         158.0       5.1
         162.0      80.2
         163.0       6.8
         164.0       3.9
         166.0       4.7
         168.0       2.0
         178.0       1.8
         182.0     100.0
         183.0       7.2
         184.0      33.1
         185.0       2.3
         197.0      21.5
         198.0       5.5
         199.0       7.3
         200.0       1.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H17 Cl N O P 0.05 ml : 0.5 ml CDCl3
    methyl diisopropylphosphoramidochloridite
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.784 B 3.619 C 1.26 J(B,P-31)=14.2HZ

         Hz     ppm     Int.
    

       1531.98   3.834     66
       1531.37   3.832     64
       1526.98   3.821     30
       1524.41   3.815    113
       1520.39   3.805     75
       1517.70   3.798    160
       1513.67   3.788    123
       1510.86   3.781    134
       1508.42   3.775     65
       1506.84   3.771    149
       1504.03   3.764     75
       1500.00   3.754    112
       1493.16   3.737     51
       1456.42   3.645     62
       1453.37   3.637   1000
       1439.21   3.602   1000
        523.68   1.311    154
        516.85   1.294    255
        511.84   1.281    346
        507.45   1.270    412
        505.13   1.264    448
        503.05   1.259    461
        500.73   1.253    456
        496.34   1.242    431
        469.12   1.174     51
        462.65   1.158     34
        462.28   1.157     34
    

in CDCl3



liquid film