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MassMS-NW-9542 methyl diisopropylphosphoramidochloridite C7H17ClNOP (Mass of molecular ion: 197)
Source Temperature: 240 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 5.1 18.0 1.1 27.0 8.3 28.0 4.0 29.0 1.6 30.0 2.3 31.0 1.2 36.0 1.9 39.0 4.4 40.0 1.0 41.0 16.5 42.0 21.7 43.0 22.3 44.0 21.0 45.0 1.3 46.0 16.2 47.0 14.5 48.0 1.3 49.0 1.2 50.0 5.8 52.0 1.9 56.0 3.0 58.0 11.8 59.0 1.9 62.0 2.6 63.0 21.2 64.0 1.0 67.0 1.1 70.0 2.9 72.0 1.9 73.0 1.9 74.0 1.8 78.0 32.4 79.0 3.4 80.0 1.4 82.0 2.1 84.0 16.0 85.0 1.2 86.0 9.7 88.0 40.4 89.0 1.7 90.0 7.9 93.0 15.8 94.0 2.7 96.0 1.4 97.0 41.4 98.0 1.6 99.0 13.5 100.0 2.2 104.0 64.7 105.0 2.8 108.0 33.6 109.0 2.8 110.0 11.6 118.0 5.5 120.0 21.2 121.0 1.0 122.0 11.3 124.0 4.6 126.0 1.1 128.0 2.5 130.0 3.0 131.0 1.0 132.0 3.9 136.0 3.7 140.0 52.5 141.0 2.4 142.0 17.4 146.0 1.1 147.0 1.5 150.0 2.3 152.0 2.6 154.0 2.7 156.0 16.5 158.0 5.1 162.0 80.2 163.0 6.8 164.0 3.9 166.0 4.7 168.0 2.0 178.0 1.8 182.0 100.0 183.0 7.2 184.0 33.1 185.0 2.3 197.0 21.5 198.0 5.5 199.0 7.3 200.0 1.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H17 Cl N O P 0.05 ml : 0.5 ml CDCl3 methyl diisopropylphosphoramidochloridite 
Assign. Shift(ppm)
A 3.784 B 3.619 C 1.26 J(B,P-31)=14.2HZ
Hz ppm Int.1531.98 3.834 66 1531.37 3.832 64 1526.98 3.821 30 1524.41 3.815 113 1520.39 3.805 75 1517.70 3.798 160 1513.67 3.788 123 1510.86 3.781 134 1508.42 3.775 65 1506.84 3.771 149 1504.03 3.764 75 1500.00 3.754 112 1493.16 3.737 51 1456.42 3.645 62 1453.37 3.637 1000 1439.21 3.602 1000 523.68 1.311 154 516.85 1.294 255 511.84 1.281 346 507.45 1.270 412 505.13 1.264 448 503.05 1.259 461 500.73 1.253 456 496.34 1.242 431 469.12 1.174 51 462.65 1.158 34 462.28 1.157 34
in CDCl3
liquid film
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