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MS-IW-7437 4-bromophthalic anhydride C8H3BrO3 (Mass of molecular ion: 226)
Source Temperature: 140 °C Sample Temperature: 110 °C Direct, 75 eV
28.0 2.1 36.0 1.2 37.0 10.6 37.5 3.6 38.0 3.9 49.0 4.6 50.0 7.2 51.0 4.1 53.0 1.6 60.0 1.0 61.0 2.5 62.0 1.3 72.0 1.2 73.0 12.0 74.0 46.7 75.0 79.8 76.0 5.7 77.0 12.7 77.5 1.2 78.0 12.1 91.0 7.9 92.0 7.7 103.0 5.4 104.0 1.1 128.0 1.1 130.0 1.2 154.0 47.7 155.0 4.0 156.0 46.5 157.0 3.1 182.0 100.0 183.0 8.0 184.0 98.7 185.0 7.6 226.0 63.2 227.0 5.7 228.0 62.1 229.0 5.7
parameter in DMSO-d6
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1H NMR 300 MHz C8 H3 Br O3 0.041 g : 0.5 ml DMSO-d6 4-bromophthalic anhydride Parameter ppm Hz
D(A) 8.344 D(B) 8.188 D(C) 8.006 J(A,B) 1.7 J(A,C) 0.4 J(B,C) 7.9
Hz ppm Int.
2504.02 8.347 927 2502.41 8.341 986 2461.46 8.205 492 2459.78 8.199 459 2453.56 8.179 648 2451.88 8.173 614 2405.47 8.018 1000 2397.57 7.992 749
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