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MassMS-IW-0780 6-methoxy-8-nitroquinoline C10H8N2O3 (Mass of molecular ion: 204)
Source Temperature: 140 °C Sample Temperature: 110 °C Direct, 75 eV
28.0 1.3 30.0 1.1 38.0 1.0 39.0 1.2 50.0 1.7 51.0 1.4 62.0 2.5 63.0 4.4 64.0 2.3 74.0 1.3 75.0 1.5 76.0 2.0 77.0 5.8 87.0 1.2 88.0 4.9 89.0 2.5 91.0 5.2 100.0 1.2 101.0 8.0 102.0 3.1 103.0 7.6 114.0 4.4 115.0 11.7 116.0 2.9 117.0 6.4 118.0 3.1 127.0 1.8 128.0 28.6 129.0 3.5 130.0 5.5 131.0 1.8 143.0 3.4 146.0 16.8 147.0 1.7 158.0 2.4 174.0 8.5 175.0 1.0 204.0 100.0 205.0 12.3 206.0 1.3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C10 H8 N2 O3 0.032 g : 0.5 ml DMSO-d6 6-methoxy-8-nitroquinoline 
Assign. Shift(ppm)
A 8.870 B 8.432 C 8.030 D 7.705 E 7.670 F 3.980
Hz ppm Int.3548.10 8.879 116 3546.51 8.875 122 3543.95 8.868 124 3542.24 8.864 121 3375.24 8.446 88 3373.78 8.442 88 3366.82 8.425 97 3365.11 8.421 90 3210.57 8.034 196 3207.76 8.027 204 3080.69 7.709 154 3077.88 7.702 148 3071.53 7.686 104 3067.26 7.675 101 3063.11 7.665 99 3058.96 7.655 94 1590.82 3.981 1000
in DMSO-d6
KBr disc
nujol mull
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