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MassMS-NW-0389 butoxycarbonylmethyl butyl phthalate C18H24O6 (Mass of molecular ion: 336)
Source Temperature: 140 °C Sample Temperature: 100 °C Direct, 75 eV
27.0 1.7 29.0 9.0 39.0 1.6 41.0 9.1 42.0 1.8 50.0 1.6 55.0 2.3 56.0 8.3 57.0 13.9 65.0 2.3 76.0 5.5 77.0 15.9 93.0 2.3 104.0 8.7 105.0 5.0 121.0 2.4 122.0 1.2 132.0 3.7 133.0 19.4 134.0 1.3 149.0 100.0 150.0 9.5 151.0 1.0 160.0 1.6 205.0 4.7 207.0 7.1 223.0 1.5 263.0 42.3 264.0 6.7 265.0 1.0 281.0 4.1 336.0 2.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C18 H24 O6 0.04 ml : 0.5 ml CDCl3 butoxycarbonylmethyl butyl phthalate 
Assign. Shift(ppm)
A 7.80 B *1 7.59 C *1 7.54 D 4.828 E 4.306 F 4.205 G 1.75 to 1.27 J 0.96 to 0.91
Hz ppm Int.705.00 7.872 73 704.44 7.866 78 701.31 7.831 157 700.38 7.821 85 699.63 7.812 79 698.50 7.800 114 697.38 7.787 111 696.00 7.772 166 695.44 7.766 226 694.50 7.755 122 691.75 7.724 223 691.13 7.717 119 687.63 7.678 53 683.75 7.635 106 680.00 7.593 358 676.44 7.553 272 674.13 7.528 229 670.81 7.491 185 432.50 4.830 1000 392.19 4.380 167 385.69 4.307 430 383.00 4.277 158 381.13 4.256 52 379.25 4.235 237 376.56 4.205 363 370.13 4.133 195 162.44 1.814 44 160.94 1.798 62 160.44 1.792 63 157.06 1.754 61 153.94 1.719 137 152.94 1.708 113 151.81 1.696 91 147.75 1.650 187 146.38 1.635 166 141.19 1.577 177 138.38 1.546 128 135.63 1.515 100 133.69 1.493 134 132.25 1.477 110 130.25 1.455 121 127.81 1.428 118 126.19 1.409 153 123.50 1.379 118 122.19 1.365 110 119.63 1.336 102 116.94 1.306 105 115.94 1.295 69 113.06 1.263 79 111.75 1.248 45 110.44 1.234 41 106.31 1.188 39 91.94 1.027 243 91.31 1.020 238 90.69 1.013 229 89.75 1.003 252 85.44 0.954 467 83.13 0.929 509 79.94 0.893 97 79.25 0.885 94 77.94 0.871 130 76.69 0.857 103 75.75 0.846 111 73.88 0.825 43
in CDCl3
CCl4 solution
liquid film
4880 A,200 M,liquid
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