-
MassMS-KW-0162 2-methylnaphth(1,2-d)oxazole C12H9NO (Mass of molecular ion: 183)
Source Temperature: 240 °C Sample Temperature: 150 °C Reservoir, 75 eV
39.0 1.5 43.0 1.0 50.0 1.5 51.0 2.2 57.0 1.2 62.0 3.3 63.0 6.2 64.0 3.7 71.0 1.5 74.0 1.7 75.0 2.4 76.0 1.3 76.5 1.2 77.0 3.5 77.5 7.3 78.0 1.1 86.0 1.7 87.0 2.6 88.0 6.6 91.5 6.8 101.0 1.2 113.0 9.6 114.0 26.7 115.0 4.8 127.0 2.9 128.0 11.1 129.0 1.7 140.0 2.0 153.0 1.2 154.0 21.0 155.0 12.1 156.0 1.4 182.0 12.9 183.0 100.0 184.0 13.5 185.0 1.1
400 MHz in CDCl3
-
1H NMR 399.65 MHz C12 H9 N O 0.05 ml : 0.5 ml CDCl3 2-methylnaphth(1,2-d)oxazole 
Assign. Shift(ppm)
A 8.431 B 7.810 C 7.57 D *1 7.56 E 7.463 F *1 7.411 G 2.576
Hz ppm Int.3374.88 8.445 133 3374.15 8.443 128 3373.66 8.442 134 3366.58 8.424 138 3365.84 8.422 135 3365.36 8.421 140 3125.00 7.820 138 3116.82 7.799 150 3030.64 7.584 218 3024.78 7.569 132 3023.56 7.566 193 3022.09 7.562 274 3016.48 7.548 103 3015.26 7.545 99 2986.33 7.473 334 2977.42 7.451 240 2969.73 7.431 115 2968.38 7.428 119 2962.77 7.414 105 2961.43 7.411 178 2960.21 7.408 116 2954.59 7.393 85 2953.25 7.390 86 1029.79 2.577 1000
in CDCl3
更多供应商
