图谱信息 供应商 相关产品
网站主页CAS数据库列表 84-85-5更多图谱4-甲氧基-1-萘酚(84-85-5)核磁图(1HNMR)

4-甲氧基-1-萘酚

产品名称 4-甲氧基-1-萘酚

CAS号84-85-5

分子式C11H10O2

分子量174.2

展开


  • Mass

    MS-NW-7880          
    4-methoxy-1-naphthol
    C11H10O2            (Mass of molecular ion:    174)
    

       Source Temperature: 180 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          15.0       1.4
          18.0       1.1
          28.0       1.1
          38.0       1.0
          39.0       2.4
          50.0       4.1
          51.0       7.3
          52.0       1.5
          53.0       1.8
          57.5       1.0
          62.0       2.2
          63.0       4.3
          65.0       1.7
          65.5       2.0
          74.0       3.0
          75.0       4.5
          76.0       6.9
          77.0      19.6
          78.0       1.6
          86.0       1.4
          87.0       5.0
          88.0       1.6
          89.0       2.2
          91.0       3.8
         101.0       2.3
         102.0       7.9
         103.0      18.1
         104.0       4.3
         105.0      13.3
         106.0       2.1
         113.0       1.5
         114.0       1.9
         115.0       5.9
         116.0       1.0
         129.0       1.0
         130.0       3.2
         131.0      23.8
         132.0       2.5
         145.0       3.1
         159.0     100.0
         160.0      11.6
         161.0       1.1
         173.0       5.8
         174.0      85.5
         175.0      10.8
         176.0       1.0
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C11 H10 O2 0.039 g : 0.5 ml DMSO-d6
    4-methoxy-1-naphthol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.59 B *1 8.12 C *1 8.09 D *2 7.498 E *2 7.479 F 6.790 G 6.772 J 3.883 J(F,G)=8.2HZ

         Hz     ppm     Int.
    

       3834.53   9.595    378
       3252.56   8.139     65
       3251.95   8.137     69
       3248.90   8.130     86
       3246.77   8.125     51
       3245.09   8.120     68
       3242.95   8.115     79
       3242.19   8.113     84
       3239.75   8.107     84
       3238.98   8.105     70
       3236.85   8.100     69
       3235.17   8.096     53
       3233.03   8.090     99
       3229.98   8.083     86
       3229.37   8.081     68
       2997.44   7.501    202
       2994.69   7.494    113
       2993.62   7.491    106
       2991.49   7.486    114
       2990.57   7.483     99
       2987.67   7.476    191
       2720.18   6.807     65
       2712.10   6.787    303
       2707.82   6.776    258
       2699.58   6.755     58
       1551.82   3.883   1000
    

KBr disc



nujol mull