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MassMS-KW-0123 trimethyl(2-((trimethylsilyl)methyl)benzyl)ammonium iodide C14H26INSi (Mass of molecular ion: 363)
Source Temperature: 180 °C Sample Temperature: 170 °C Direct, 75 eV
15.0 2.6 27.0 1.0 28.0 1.8 29.0 1.5 30.0 6.7 39.0 1.5 41.0 1.0 42.0 6.8 43.0 7.0 44.0 3.1 45.0 9.7 50.0 1.0 51.0 1.9 53.0 1.5 57.0 3.0 58.0 39.7 59.0 21.4 66.0 1.0 72.0 1.5 73.0 100.0 74.0 8.6 75.0 5.2 77.0 3.3 78.0 4.0 81.0 1.6 91.0 1.3 102.0 2.2 103.0 5.2 104.0 19.9 105.0 5.0 115.0 1.8 117.0 1.8 119.0 2.3 121.0 1.3 127.0 4.0 128.0 6.7 131.0 1.9 133.0 2.4 135.0 1.8 142.0 3.2 145.0 5.7 146.0 1.6 147.0 4.1 148.0 1.8 149.0 6.5 159.0 1.4 161.0 16.8 162.0 4.3 163.0 1.9 176.0 3.4 177.0 93.9 178.0 16.8 179.0 4.5 185.0 7.7 206.0 1.4 221.0 3.6 289.0 3.2
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C14 H26 I N Si 0.035 g : 0.5 ml DMSO-d6 trimethyl(2-((trimethylsilyl)methyl)benzyl)ammonium iodide 
Assign. Shift(ppm)
A 7.487 B 7.391 C 7.21 D 7.18 E 4.541 F 3.092 G 2.408 J -0.042
Hz ppm Int.2996.83 7.499 25 2995.85 7.497 27 2989.01 7.480 29 2988.16 7.477 31 2955.32 7.395 30 2953.98 7.392 30 2947.75 7.376 21 2888.92 7.229 21 2882.57 7.213 28 2881.35 7.210 33 2873.66 7.191 46 2865.72 7.171 30 2864.62 7.168 27 1814.82 4.542 120 1235.96 3.093 492 962.52 2.409 123 -13.54 -0.033 81 -16.59 -0.041 1000 -19.89 -0.049 77
in DMSO-d6
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