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MS-NW-0100 1,5-naphthalenediol C10H8O2 (Mass of molecular ion: 160)
Source Temperature: 210 °C Sample Temperature: 0 °C Direct, 75 eV
39.0 1.9 50.0 2.7 51.0 6.9 52.0 1.4 53.0 1.1 62.0 1.4 63.0 2.4 65.0 1.5 65.5 1.9 66.0 2.1 74.0 2.1 75.0 2.2 76.0 2.6 77.0 10.0 78.0 3.3 80.0 4.3 102.0 4.3 103.0 9.8 104.0 4.8 114.0 1.0 115.0 3.5 131.0 58.1 132.0 12.8 133.0 1.1 159.0 3.8 160.0 100.0 161.0 11.3 162.0 1.0
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C10 H8 O2 0.031 g : 0.5 ml DMSO-d6 1,5-naphthalenediol Assign. Shift(ppm)
A 9.92 B 7.588 C 7.224 D 6.852
Hz ppm Int.
3962.71 9.916 363 3046.88 7.624 26 3046.11 7.622 26 3036.96 7.600 881 3028.56 7.579 982 2895.36 7.245 554 2887.42 7.225 950 2879.49 7.206 563 2742.31 6.862 1000 2734.83 6.844 916
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