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MassMS-NW-8342 phenylphosphonic dichloride C6H5Cl2OP (Mass of molecular ion: 194)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
27.0 3.1 28.0 1.5 36.0 4.0 37.0 1.2 38.0 2.3 39.0 3.8 47.0 15.2 49.0 1.1 50.0 18.9 51.0 46.6 52.0 2.3 62.0 1.0 63.0 1.1 65.0 6.9 68.0 1.0 73.0 1.2 74.0 6.0 75.0 5.5 76.0 5.6 77.0 95.6 78.0 6.4 80.0 1.0 93.0 4.6 101.0 1.7 103.0 1.2 107.0 1.4 112.0 4.9 114.0 1.6 159.0 100.0 160.0 6.7 161.0 32.5 162.0 2.2 194.0 40.9 195.0 2.8 196.0 26.2 197.0 1.8 198.0 4.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H5 Cl2 O P 0.05 ml : 0.5 ml CDCl3 phenylphosphonic dichloride 
Assign. Shift(ppm)
A 7.975 B 7.700 C 7.598
Hz ppm Int.3201.05 8.010 593 3199.83 8.007 659 3199.10 8.005 352 3198.49 8.004 339 3194.70 7.994 233 3192.87 7.990 772 3191.41 7.986 678 3183.11 7.965 578 3181.88 7.962 656 3181.03 7.960 356 3180.54 7.959 337 3176.76 7.949 223 3174.93 7.945 748 3173.34 7.941 683 3087.28 7.725 190 3086.06 7.722 196 3084.96 7.720 200 3083.62 7.716 134 3081.91 7.712 153 3079.83 7.707 486 3077.76 7.702 483 3075.56 7.696 172 3073.61 7.691 220 3072.39 7.688 356 3071.04 7.685 349 3069.82 7.682 340 3068.60 7.679 182 3047.00 7.625 162 3045.65 7.621 532 3045.29 7.620 541 3043.82 7.617 279 3038.82 7.604 922 3037.48 7.601 1000 3036.01 7.597 319 3031.01 7.585 867 3025.15 7.570 166 3023.44 7.566 339
in CDCl3
liquid film
4880 A,200 M,liquid
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