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MassMS-IW-8385 tributyl(cyanomethyl)phosphonium chloride C14H29ClNP (Mass of molecular ion: 277)
Source Temperature: 170 °C Sample Temperature: 170 °C Direct, 75 eV
17.0 1.4 18.0 7.9 26.0 2.5 27.0 12.4 28.0 7.9 29.0 35.5 30.0 1.0 35.0 3.3 36.0 37.3 37.0 1.2 38.0 12.4 39.0 10.9 40.0 3.2 41.0 46.6 42.0 4.5 43.0 4.5 44.0 1.3 45.0 4.4 46.0 1.9 47.0 4.9 48.0 2.8 49.0 1.2 50.0 1.0 51.0 1.8 52.0 1.1 53.0 4.3 54.0 8.5 55.0 29.9 56.0 10.1 57.0 11.6 58.0 2.3 59.0 9.7 60.0 2.7 61.0 30.1 62.0 33.9 63.0 3.2 67.0 2.2 68.0 1.2 69.0 3.1 70.0 1.5 71.0 5.7 72.0 37.0 73.0 13.0 74.0 4.8 75.0 12.5 76.0 100.0 77.0 5.0 78.0 6.4 81.0 1.7 82.0 1.9 83.0 6.6 85.0 3.8 86.0 7.4 87.0 30.1 88.0 9.0 89.0 9.3 90.0 48.2 91.0 3.2 92.0 7.8 95.0 1.3 96.0 4.2 97.0 2.3 98.0 1.4 99.0 2.7 100.0 10.2 101.0 94.3 102.0 17.9 103.0 10.7 104.0 17.1 105.0 2.0 113.0 2.4 114.0 7.8 115.0 43.5 116.0 27.0 117.0 5.3 118.0 21.9 119.0 1.7 120.0 3.5 126.0 1.4 127.0 1.7 128.0 58.1 129.0 38.3 130.0 9.6 131.0 14.8 132.0 4.0 134.0 2.3 140.0 1.0 141.0 1.1 142.0 8.8 143.0 36.0 144.0 4.8 145.0 14.8 146.0 6.8 147.0 2.5 156.0 24.0 157.0 18.6 158.0 7.7 159.0 2.4 160.0 8.8 161.0 2.3 162.0 2.1 170.0 18.5 171.0 4.8 173.0 8.1 174.0 1.9 184.0 19.1 185.0 18.5 186.0 4.0 187.0 13.3 188.0 1.6 189.0 3.0 198.0 1.2 199.0 2.4 201.0 1.3 202.0 5.4 203.0 1.2 212.0 45.6 213.0 6.9 226.0 6.1 240.0 11.5 241.0 49.5 242.0 15.2 243.0 1.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H29 Cl N P 0.046 g : 0.5 ml CDCl3 tributyl(cyanomethyl)phosphonium chloride 
Assign. Shift(ppm)
A 5.061 B 2.679 C 1.681 D 1.557 E 1.001
Hz ppm Int.2030.52 5.081 140 2014.89 5.042 139 1086.18 2.718 98 1080.69 2.705 61 1077.64 2.697 80 1072.75 2.685 139 1069.46 2.676 142 1064.70 2.665 84 1062.13 2.658 63 1058.59 2.649 46 1056.03 2.643 113 686.28 1.718 61 684.94 1.714 63 678.47 1.698 113 674.07 1.687 84 670.65 1.679 128 665.77 1.666 68 662.48 1.658 98 659.67 1.651 50 654.42 1.638 38 639.89 1.602 38 632.69 1.584 134 625.37 1.565 216 618.04 1.547 202 610.84 1.529 109 407.10 1.019 496 399.90 1.001 1000 392.58 0.983 466
in CDCl3
KBr disc
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