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2-环己烯醇

CAS号822-67-3

分子式C6H10O

分子量98.14

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  • Mass

    MS-KW-0253          
    2-cyclohexen-1-ol
    C6H10O              (Mass of molecular ion:     98)
    

       Source Temperature: 230 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       1.8
          17.0       2.6
          18.0       9.8
          26.0       3.3
          27.0      20.0
          28.0       4.6
          29.0      11.2
          31.0       4.2
          37.0       2.4
          38.0       5.0
          39.0      32.3
          40.0       7.0
          41.0      28.7
          42.0      16.9
          43.0      16.1
          44.0       4.5
          47.0       1.0
          49.0       1.3
          50.0       9.0
          51.0      14.2
          52.0      10.0
          53.0      10.2
          54.0      10.8
          55.0      30.2
          56.0       5.3
          57.0      13.6
          58.0       1.1
          62.0       1.1
          63.0       2.2
          65.0       5.7
          66.0       1.9
          67.0       9.0
          68.0       3.6
          69.0      22.9
          70.0     100.0
          71.0       5.2
          74.0       2.2
          75.0       1.2
          77.0      33.9
          78.0      13.8
          79.0      78.4
          80.0      38.9
          81.0       6.6
          82.0       2.3
          83.0      35.3
          84.0       2.0
          95.0       1.2
          97.0      29.7
          98.0      35.5
          99.0       2.8
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6H10O 0.05 ml : 0.5 ml CDCl3
    2-cyclohexen-1-ol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.800 B 5.739 C 4.179 D 2.8 E *1 2.02 F *1 1.86 G *2 1.74 J *2 1.61 K *2 1.57 assigned by C-H COSY

         Hz     ppm     Int.
    

       2329.23   5.827    181
       2328.13   5.824    182
       2325.81   5.818    306
       2324.59   5.815    288
       2322.27   5.809    184
       2321.17   5.807    175
       2319.22   5.802    314
       2318.00   5.799    326
       2315.68   5.793    570
       2314.46   5.790    569
       2312.14   5.784    336
       2311.04   5.781    329
       2300.66   5.755    311
       2298.71   5.750    516
       2295.90   5.743    483
       2293.71   5.738    250
       2288.70   5.725    249
       2285.77   5.718    260
       2283.57   5.713    145
       1672.49   4.184    395
       1671.51   4.182    383
       1669.44   4.176    344
       1668.46   4.174    304
       1109.50   2.776   1000
        824.83   2.064     86
        822.88   2.059    104
        821.54   2.055    107
        819.46   2.050    121
        817.51   2.045    114
        815.56   2.040    106
        812.38   2.033    129
        810.31   2.027    173
        808.23   2.022    163
        806.89   2.019    237
        804.94   2.014    249
        803.23   2.010    316
        801.40   2.005    306
        799.44   2.000    316
        797.49   1.995    279
        795.54   1.990    177
        793.95   1.986    216
        792.00   1.982    208
        790.41   1.978    180
        788.58   1.973    241
        786.38   1.968    293
        783.70   1.961    323
        782.84   1.959    294
        780.40   1.953    270
        778.69   1.948    193
        776.98   1.944    159
        770.39   1.928    105
        768.32   1.922    124
        764.78   1.913    130
        761.11   1.904    192
        758.67   1.898    193
        755.74   1.891    159
        753.55   1.885    185
        749.64   1.876    283
        744.76   1.863    291
        740.12   1.852    297
        735.11   1.839    216
        727.18   1.819     73
        716.92   1.794     62
        709.48   1.775    121
        703.62   1.760    261
        701.05   1.754    192
        699.10   1.749    235
        693.00   1.734    296
        687.50   1.720    209
        685.06   1.714    202
        682.74   1.708    192
        678.84   1.699     97
        676.40   1.692    104
        656.74   1.643    194
        654.18   1.637     98
        650.40   1.627    202
        647.59   1.620    320
        645.15   1.614    311
        641.12   1.604    355
        639.04   1.599    410
        638.07   1.597    415
        634.89   1.589    468
        633.43   1.585    429
        632.09   1.582    433
        630.99   1.579    361
        629.16   1.574    432
        626.96   1.569    363
        623.42   1.560    226
        621.22   1.554    194
        620.00   1.551    206
        617.56   1.545    179
        614.26   1.537    169
        612.07   1.531     99
        610.72   1.528     90
        607.67   1.520     71
        605.11   1.514     75
    

in CDCl3



liquid film