-
MassMS-IW-3661 1-hydroxy-4-nitroanthraquinone C14H7NO5 (Mass of molecular ion: 269)
Source Temperature: 140 °C Sample Temperature: 100 °C Direct, 75 eV
18.0 2.4 28.0 1.3 30.0 1.8 39.0 2.0 50.0 3.6 51.0 2.5 53.0 1.4 61.0 1.2 62.0 4.1 63.0 6.5 65.0 1.3 69.0 1.9 69.5 3.5 74.0 3.5 75.0 4.7 76.0 5.1 77.0 4.9 83.0 1.3 86.0 2.4 87.0 3.7 88.0 1.9 89.0 5.5 90.0 1.4 91.0 2.5 98.0 1.7 99.0 1.8 101.0 2.9 104.0 1.7 105.0 2.8 110.0 1.0 111.0 1.5 112.0 1.2 113.0 5.7 126.0 2.2 127.0 6.7 128.0 1.2 129.0 1.3 137.0 4.3 138.0 7.0 139.0 42.3 140.0 5.4 155.0 4.5 167.0 11.1 168.0 1.6 171.0 1.2 183.0 12.6 184.0 1.8 195.0 11.8 196.0 2.3 211.0 22.8 212.0 3.5 222.0 1.5 223.0 2.5 239.0 38.6 240.0 6.3 241.0 1.0 253.0 1.3 269.0 100.0 270.0 16.0 271.0 2.2
400 MHz in DMSO-d6
-
1H NMR 399.65 MHz C14 H7 N O5 saturated in DMSO-d6 1-hydroxy-4-nitroanthraquinone 
Assign. Shift(ppm)
A 8.251 B 8.129 C 8.093 D *1 8.00 E *1 7.98 F 7.546
Hz ppm Int.3302.49 8.264 395 3299.93 8.258 305 3298.95 8.255 277 3297.24 8.251 271 3295.04 8.245 328 3293.46 8.241 503 3291.50 8.236 62 3290.65 8.234 62 3289.67 8.232 90 3254.03 8.143 379 3251.95 8.137 271 3249.63 8.132 282 3248.29 8.128 311 3247.80 8.127 294 3247.44 8.126 299 3244.87 8.120 503 3242.80 8.115 68 3242.43 8.114 68 3241.82 8.112 79 3239.14 8.105 915 3230.10 8.083 989 3205.93 8.022 68 3204.96 8.020 79 3204.59 8.019 85 3202.51 8.014 181 3201.29 8.011 79 3200.93 8.010 79 3200.44 8.009 90 3199.71 8.007 90 3197.27 8.001 605 3195.43 7.996 859 3191.89 7.987 960 3188.60 7.979 701 3186.65 7.974 418 3181.15 7.960 119 3178.96 7.955 79 3020.26 7.558 1000 3011.35 7.535 944
in DMSO-d6
KBr disc
nujol mull
更多供应商
