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3-甲氧基-4-硝基苯甲醇

产品名称 3-甲氧基-4-硝基苯甲醇

CAS号80866-88-2

分子式C8H9NO4

分子量183.16


  • Mass

    MS-NW-8075          
    3-methoxy-4-nitrobenzyl alcohol
    C8H9NO4             (Mass of molecular ion:    183)
    

       Source Temperature: 170 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          15.0       5.0
          17.0       1.6
          18.0       7.7
          26.0       1.3
          27.0       8.1
          28.0       7.4
          29.0       9.1
          30.0       7.4
          31.0      11.2
          37.0       2.3
          38.0       6.3
          39.0      28.3
          40.0       6.9
          41.0       9.3
          42.0       1.4
          43.0       3.1
          45.0       2.0
          47.0       1.1
          50.0      12.6
          51.0      26.7
          52.0      12.2
          53.0      24.9
          54.0       5.3
          55.0       8.8
          59.0       4.9
          61.0       2.6
          62.0       8.4
          63.0      20.8
          64.0       7.1
          65.0      39.0
          66.0      35.4
          67.0       9.7
          68.0       2.7
          69.0       2.1
          74.0       5.8
          75.0       6.2
          76.0       9.5
          77.0      68.1
          78.0      26.0
          79.0      43.3
          80.0      59.7
          81.0      14.3
          82.0       8.4
          83.0       1.0
          89.0      39.4
          90.0       7.1
          91.0       9.3
          92.0       7.6
          93.0      14.3
          94.0      25.6
          95.0       5.6
          96.0       5.6
          97.0       9.9
          98.0       1.2
         104.0       2.2
         105.0      40.1
         106.0      15.6
         107.0      12.8
         108.0      39.5
         109.0      12.9
         110.0       3.5
         119.0       6.0
         120.0       2.8
         121.0       8.9
         122.0       6.2
         123.0       2.4
         124.0      19.0
         125.0       2.3
         134.0       1.1
         135.0       5.4
         136.0      28.1
         137.0       5.8
         138.0       1.7
         150.0       1.0
         151.0       1.1
         152.0       3.1
         153.0      16.0
         154.0       4.0
         166.0       3.4
         167.0       2.3
         182.0       1.7
         183.0     100.0
         184.0      12.4
         185.0       1.5
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C8 H9 N O4 0.040 g : 0.5 ml CDCl3
    3-methoxy-4-nitrobenzyl alcohol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.820 B 7.135 C 6.960 D 4.76 E 3.955 F 2.53

         Hz     ppm     Int.
    

        704.44   7.866    132
        696.25   7.775    160
        639.19   7.138    125
        638.75   7.133    127
        628.50   7.018     57
        627.81   7.010     91
        627.00   7.001     79
        626.19   6.992     77
        619.50   6.918     74
        618.63   6.908     66
        617.88   6.900     64
        617.19   6.892     40
        426.81   4.766    165
        354.25   3.956   1000
    

in CDCl3



KBr disc



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