2-氯-5-硝基苄醇

Mass

MS-NW-7257          
2-chloro-5-nitrobenzyl alcohol
C7H6ClNO3           (Mass of molecular ion:    187)

   Source Temperature: 140 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      17.0       1.4
      18.0       5.4
      26.0       1.5
      27.0       6.6
      28.0       5.7
      29.0      12.7
      30.0       9.8
      31.0      19.7
      36.0       1.8
      37.0       6.0
      38.0       8.2
      39.0      17.3
      40.0       1.7
      43.0       1.9
      46.0       1.8
      49.0       3.1
      50.0      30.7
      51.0      61.2
      52.0       9.9
      53.0       3.9
      55.0       3.1
      60.0       1.2
      61.0       6.7
      62.0      10.7
      63.0      21.0
      64.0       3.7
      65.0      14.4
      66.0       3.7
      72.0       1.4
      73.0      11.6
      74.0      24.8
      75.0      57.5
      76.0      16.9
      77.0     100.0
      78.0      30.2
      79.0       2.4
      84.0       3.7
      85.0       5.6
      86.0       4.2
      87.0       5.9
      88.0       1.9
      89.0      10.9
      90.0       2.3
      92.0       2.0
      93.0       2.2
      94.0      11.1
      95.0       1.0
      97.0       2.8
      98.0       1.2
      99.0       4.0
     100.0       1.6
     101.0       1.6
     103.0       1.5
     104.0       4.5
     105.0      17.8
     106.0       9.1
     107.0       1.7
     109.0       1.5
     110.0       8.2
     111.0      45.5
     112.0      22.0
     113.0      17.9
     114.0       6.9
     115.0       2.1
     121.0       2.6
     122.0       5.5
     123.0      65.6
     124.0      34.3
     125.0      24.0
     126.0       5.1
     127.0       1.3
     128.0       3.2
     129.0       1.5
     130.0       1.1
     138.0       3.1
     139.0      19.5
     140.0      24.6
     141.0      58.6
     142.0      18.8
     143.0      19.4
     144.0       3.8
     150.0       5.6
     151.0       1.6
     152.0      47.0
     153.0       4.4
     155.0       3.1
     157.0       2.1
     158.0      18.2
     159.0       1.9
     160.0       6.2
     169.0       2.7
     170.0      15.7
     171.0       4.8
     172.0       5.4
     173.0       1.4
     184.0       3.8
     185.0       2.9
     186.0      12.3
     187.0      87.1
     188.0      11.2
     189.0      28.7
     190.0       2.8

Assign. Shift(ppm) A 8.436 B 8.088 C 7.514 D 4.861 E 2.52

     Hz     ppm     Int.

   3373.54   8.442    393
   3372.68   8.440    615
   3372.07   8.438    401
   3370.24   8.433    637
   3238.89   8.105    267
   3238.28   8.103    449
   3237.67   8.102    257
   3236.08   8.098    269
   3235.47   8.096    430
   3234.86   8.095    241
   3232.79   8.090     31
   3232.18   8.088     30
   3230.22   8.083    289
   3229.61   8.082    476
   3229.00   8.080    276
   3227.42   8.076    294
   3226.81   8.075    469
   3226.20   8.073    260
   3007.45   7.526   1000
   2998.78   7.504    941
   1943.97   4.865    626
   1941.77   4.859    652
   1006.84   2.520    257