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MassMS-NW-6675 3-methyl-4-nitrobenzyl alcohol C8H9NO3 (Mass of molecular ion: 167)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
18.0 2.6 27.0 5.8 28.0 7.3 29.0 4.3 30.0 3.5 31.0 6.8 32.0 1.0 37.0 1.1 38.0 2.9 39.0 17.0 40.0 2.5 41.0 10.7 43.0 4.1 50.0 5.2 51.0 13.2 52.0 4.7 53.0 9.0 54.0 1.9 55.0 4.6 61.0 1.4 62.0 4.1 63.0 11.1 64.0 3.8 65.0 23.9 66.0 5.1 67.0 5.9 68.0 1.1 74.0 2.2 75.0 2.1 76.0 2.3 77.0 44.3 78.0 10.7 79.0 4.9 80.0 3.1 81.0 3.1 86.0 1.1 87.0 1.1 89.0 7.2 90.0 3.4 91.0 38.4 92.0 28.5 93.0 8.6 94.0 6.5 95.0 1.9 102.0 2.1 103.0 15.4 104.0 5.7 105.0 2.9 106.0 2.4 107.0 3.5 108.0 1.5 118.0 1.1 119.0 4.3 120.0 26.7 121.0 5.0 122.0 4.2 132.0 3.5 134.0 1.4 135.0 1.4 148.0 2.2 150.0 100.0 151.0 10.8 152.0 3.0 166.0 1.2 167.0 13.0 168.0 1.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H9 N O3 0.048 g : 0.5 ml CDCl3 3-methyl-4-nitrobenzyl alcohol 
Assign. Shift(ppm)
A 7.932 B 7.33 C 7.29 D 4.740 E 2.581 F 2.51
Hz ppm Int.715.56 7.990 151 712.69 7.958 37 709.44 7.922 28 706.63 7.891 202 656.31 7.329 263 655.56 7.320 231 653.69 7.299 136 650.13 7.260 99 649.56 7.253 99 648.25 7.239 67 424.56 4.741 542 231.19 2.582 1000 225.19 2.515 174
in CDCl3
KBr disc
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