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MassMS-KW-0525 alpha-allylbenzyl alcohol C10H12O (Mass of molecular ion: 148)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
18.0 2.0 27.0 3.0 29.0 1.9 39.0 6.3 41.0 3.7 50.0 3.0 51.0 10.0 52.0 2.3 53.0 1.8 63.0 2.1 64.0 1.8 65.0 1.9 74.0 1.0 75.0 1.0 76.0 1.1 77.0 27.3 78.0 4.6 79.0 56.8 80.0 3.8 91.0 2.4 105.0 6.6 106.0 1.2 107.0 100.0 108.0 8.0 115.0 5.9 127.0 2.7 128.0 6.0 129.0 10.8 130.0 9.3 131.0 1.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C10H12O 0.05 ml : 0.5 ml CDCl3 1-phenyl-3-buten-1-ol 
Assign. Shift(ppm)
A 7.30 B 7.23 C 5.756 D 5.081 E 5.057 F 4.643 G 3.21 J 2.458
Hz ppm Int.2925.66 7.319 88 2921.27 7.308 1000 2917.36 7.298 707 2916.39 7.295 708 2915.65 7.294 606 2912.85 7.287 79 2910.53 7.281 63 2908.70 7.276 62 2907.48 7.273 71 2900.40 7.255 39 2897.47 7.248 55 2896.12 7.245 127 2892.71 7.236 127 2891.48 7.233 127 2890.26 7.230 86 2889.41 7.228 69 2887.46 7.223 180 2885.38 7.218 59 2884.65 7.216 54 2883.06 7.212 77 2881.84 7.209 58 2878.91 7.202 42 2322.27 5.809 55 2315.31 5.792 108 2312.02 5.784 60 2308.11 5.774 59 2305.06 5.766 170 2298.10 5.749 173 2294.93 5.741 68 2291.02 5.731 68 2287.97 5.724 130 2280.89 5.706 65 2042.36 5.109 84 2040.90 5.106 168 2038.82 5.100 203 2028.45 5.074 115 2027.35 5.072 214 2026.25 5.069 184 2025.27 5.066 210 2018.19 5.049 111 2017.09 5.046 202 2016.12 5.044 159 2015.02 5.041 132 2013.92 5.038 68 1862.43 4.659 71 1855.84 4.643 128 1849.25 4.626 70 1282.11 3.208 116 996.59 2.493 22 990.85 2.479 96 989.51 2.476 177 988.41 2.473 170 986.82 2.469 96 982.43 2.458 330 981.33 2.455 275 979.99 2.452 112 976.45 2.443 131 975.35 2.440 197 974.25 2.437 127
in CDCl3
Liquid film
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