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MassMS-NW-4899 N-methyl-N-nitroso-p-toluenesulfonamide C8H10N2O3S (Mass of molecular ion: 214)
Source Temperature: 240 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 4.8 18.0 1.9 27.0 1.3 28.0 18.8 29.0 1.7 30.0 2.5 38.0 1.1 39.0 9.2 41.0 2.7 50.0 2.4 51.0 3.9 52.0 1.2 53.0 1.0 62.0 1.7 63.0 5.8 64.0 1.6 65.0 21.1 66.0 1.3 77.0 4.1 78.0 1.1 79.0 3.8 89.0 5.2 90.0 2.8 91.0 100.0 92.0 15.2 93.0 1.0 107.0 9.9 108.0 1.3 121.0 2.4 122.0 4.3 139.0 1.3 155.0 35.1 156.0 3.1 157.0 1.9 185.0 1.9 186.0 31.2 187.0 3.4 188.0 1.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H10 N2 O3 S 0.050 g : 0.5 ml CDCl3 N-methyl-N-nitroso-p-toluenesulfonamide 
Assign. Shift(ppm)
A 7.86 B 7.38 C 3.117 D 2.453
Hz ppm Int.708.88 7.916 95 708.56 7.912 99 706.88 7.893 35 702.31 7.842 42 700.19 7.819 149 665.13 7.427 107 664.44 7.419 120 663.75 7.412 71 663.00 7.403 45 662.31 7.396 34 658.44 7.352 27 657.69 7.344 36 657.13 7.338 55 656.44 7.330 88 655.75 7.322 73 279.25 3.119 1000 219.69 2.453 392
in CDCl3
CCl4 solution
KBr disc
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