2-氨基-3-氯-5-三氟甲基吡啶

Mass

MS-IW-2630          
3-chloro-5-trifluoromethyl-2-pyridylamine
C6H4ClF3N2          (Mass of molecular ion:    196)

   Source Temperature: 230 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      28.0      10.8
      31.0       3.1
      36.0       1.2
      37.0       4.5
      38.0       3.8
      39.0       1.6
      40.0       1.4
      42.0       1.1
      43.0       1.2
      47.0       1.1
      48.0       1.8
      49.0       1.6
      50.0       4.1
      51.0       2.0
      52.0       5.0
      53.0       2.3
      56.0       1.8
      57.0       4.4
      60.0       1.0
      62.0       2.3
      63.0       3.2
      64.0       7.2
      65.0       7.8
      66.0       2.1
      68.0       1.1
      69.0       9.5
      70.0       1.2
      71.0       2.7
      72.0       1.9
      73.0       4.0
      74.0       2.2
      75.0       7.6
      76.0       1.9
      82.0       2.0
      83.0       1.0
      84.0       2.1
      85.0       1.3
      86.0       1.0
      87.0       3.1
      88.0       1.9
      89.0       3.4
      90.0       2.1
      91.0       4.6
      92.0       2.4
      93.0       1.8
      94.0       1.6
      98.0       2.8
      99.0       1.8
     100.0       2.1
     106.0       1.7
     107.0       7.3
     113.0       1.6
     114.0      14.8
     115.0       2.1
     119.0       4.0
     121.0       1.7
     122.0       1.9
     123.0       1.5
     132.0       2.2
     133.0       2.1
     134.0       5.8
     141.0      48.2
     142.0       4.1
     143.0       1.2
     146.0       3.0
     148.0       2.4
     149.0       2.7
     150.0       6.9
     151.0       1.2
     152.0       2.1
     157.0       1.0
     161.0      26.3
     162.0       2.0
     168.0       2.8
     169.0      23.9
     170.0       2.3
     171.0       7.8
     175.0       2.5
     177.0      17.7
     178.0       1.3
     179.0       5.4
     196.0     100.0
     197.0       7.8
     198.0      32.9
     199.0       2.3

Assign. Shift(ppm) A 8.24 B 7.700 C 5.61

     Hz     ppm     Int.

   3292.36   8.239    590
   3078.37   7.703   1000
   3076.54   7.699    985
   2283.81   5.715     21
   2283.08   5.713     22
   2282.10   5.711     23
   2281.86   5.710     23
   2281.25   5.709     23
   2242.68   5.612    326
   2208.13   5.526     26
   2207.76   5.525     25
   2206.42   5.521     23
   2205.44   5.519     22
   2205.08   5.518     22