2-氨基吡啶

Mass

MS-NW-1534          
2-pyridinamine
C5H6N2              (Mass of molecular ion:     94)

   Source Temperature: 240 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      26.0       2.1
      27.0       2.1
      28.0      12.7
      37.5       5.0
      38.0       9.0
      39.0      20.6
      40.0      11.8
      41.0      23.8
      42.0       2.6
      43.0       1.9
      47.0       2.7
      49.0       1.0
      50.0       5.2
      51.0       7.3
      52.0       4.9
      53.0       1.2
      54.0       2.2
      63.0       1.0
      64.0       2.1
      65.0       3.1
      66.0      12.4
      67.0      75.7
      68.0       4.7
      78.0       1.6
      93.0       4.5
      94.0     100.0
      95.0       6.5

Assign. Shift(ppm) A 8.049 B 7.379 C 6.605 D 6.469 E 4.63 J(A,B)=1.9HZ J(A,C)=5.1HZ J(A,D)=1.0HZ J(B,C)=7.3HZ J(B,D)=8.3HZ J(C,D)=1.0HZ

     Hz     ppm     Int.

    725.13   8.097    241
    724.19   8.087    268
    723.19   8.075    296
    722.31   8.066    270
    719.94   8.039    277
    719.13   8.030    301
    718.13   8.019    317
    717.25   8.009    285
    670.63   7.489    395
    668.69   7.467    382
    663.38   7.408    500
    662.38   7.396    523
    661.44   7.386    492
    660.44   7.375    480
    655.19   7.316    589
    653.25   7.294    682
    598.00   6.678    485
    597.00   6.666    586
    592.94   6.621    446
    591.94   6.610    574
    590.81   6.597    471
    589.81   6.586    469
    585.75   6.541    427
    584.75   6.530    492
    584.00   6.521    628
    583.00   6.510   1000
    582.06   6.500    491
    575.75   6.429    490
    574.81   6.419    816
    573.81   6.407    421
    414.56   4.629    206