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网站主页CAS数据库列表 78-86-4更多图谱氯代仲丁烷(78-86-4)核磁图(1HNMR)

氯代仲丁烷

产品名称 氯代仲丁烷

CAS号78-86-4

分子式C4H9Cl

分子量92.57

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  • Mass

    MS-NW-0940          
    2-chlorobutane
    C4H9Cl              (Mass of molecular ion:     92)
    

       Source Temperature: 280 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       1.4
          18.0       1.3
          26.0       5.4
          27.0      37.1
          28.0      12.6
          29.0      39.3
          30.0       1.0
          36.0       2.4
          37.0       1.4
          38.0       2.3
          39.0      17.3
          40.0       2.6
          41.0      64.1
          42.0       3.6
          43.0       1.7
          49.0       2.8
          50.0       2.5
          51.0       2.2
          53.0       2.4
          55.0       9.3
          56.0      92.6
          57.0     100.0
          58.0       4.5
          61.0       1.1
          62.0      13.2
          63.0      44.1
          64.0       5.1
          65.0      13.9
          76.0       1.0
          77.0       5.5
          79.0       1.7
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C4 H9 Cl 0.04 ml : 0.5 ml CDCl3
    2-chlorobutane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.972 B 1.71 C 1.502 D 1.024

         Hz     ppm     Int.
    

        365.88   4.086     55
        359.44   4.014     96
        353.31   3.945    106
        346.75   3.872     64
        171.44   1.915     35
        170.25   1.901     33
        165.44   1.848     43
        164.69   1.839     52
        163.38   1.825    136
        158.88   1.775     47
        157.38   1.758    149
        156.06   1.743    196
        151.44   1.691     56
        149.63   1.671    182
        148.63   1.660     73
        145.38   1.624     40
        142.81   1.595     92
        137.69   1.538   1000
        135.50   1.513     49
        131.19   1.465    938
        129.13   1.442     45
         98.06   1.095    289
         91.13   1.018    510
         83.56   0.934    182
         82.63   0.923    106
    

in CDCl3



CCl4 solution



liquid film